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← Document results/DEP Box 28/GCMS X 1/4/02 A 1/25/02
Document / 19 pages

GCMS analysis results for sample AE00027, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00027 analyzed on February 7, 2002.

NYC-WTC_000050735–000050753

Folder label: “GCMS X 1/4/02 A 1/25/02

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Scanned page image, NYC-WTC_000050741
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NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02JAN25\00027.D Vial: 3 Acq On : 25 Jan 2002 4:47 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C: \DATABASE\WILEY7N . L ********************************************************************* Peak Number 1 Dichloroacetonitrile $$ Ace... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 3.49 0.09 ug/L 39469 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 74 2 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 64 3 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 64 4 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 64 Abundance Scan 10 (3.488 min): 00027.D (-) m/z 74.00 100.00% 74

82 5000 47 / ‘11• -mmP 38 3.50 3.60 3.70 3.80 3.90 •■i■ ■‘' r1 1 ' ‘ 1 11 I ■ I..1 । 1 1 1 ■ r1 TEt • TT"’"’ । । । । । । । । > m/2 82.00 53.05% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 74 82 A /1 fi 1111111111 r n m... 5000 3.50 3.60 3.70 3.80 3.90 47 m/z 83.95 34.88% 35

miz-> —2.,. ..,...p—.lp.■ 1. 1. mM ' r 1 10 20 30 40 50 60 70 ‘11 80 90 ।.. 11198.. 100 110 _----- —)

Abundance #11643: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 74 < • ■ ' | ‘ | ■ ■ ■ ■ | ‘ ‘ | ■ i i । | . . ■ ■

47 82 3.50 3.60 3.70 3.80 3.90 5000 m/z 76.00 29.33%

38 I I ' ' T-t-p-r-r-r-p-r-r-r-p- I _________ L , 95 102 108 "IB TTTurri I ' ' 1 1 1 11 miz->_______ 10 20 30 40 50 60 70 80 90 100 110 Abundance #11644: Acetonitrile, dichloro- 74 3.50 3.60 3.70 3.80 3.90 35 m/z 47.00 25.28% 5000 82 47

1 1 I... .. '."T"’ ''' 1,1 1 1 ‘IIIII’III T-p 1 ' i ' ’ ' 1 i ' ■ 1 ■ i ' 1 m/z—> 10 20 30 40 50 60 70 80 90 100 110 3.50 3.60 3.70 3.80 3.90

00027.D SCAN508.M Mon Jan 28 09:49:29 2002 Page 3

NYC-WTC_000050741

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NYC-WTC_000050741Source: NYC Law Department, mirrored locally

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