GCMS results for sample AE00561, Jan 17 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\00561.D Vial: 5 Acq On : 15 Jan 2002 4:50 pm Operator: ’ Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Dichloroacetonitrile $$ Ace... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

3.49 0.16 ug/L 48707 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 83 2 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 83 3 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 83 4 Acetonitrile, dichloro-_______________ 109 C2HC12N 003018-12-0 64 Abundance Scan 10 (3.488 min): 00561 .D (-) m/z 74.00 100.00% 74

82 5000 47 / .............. 38 3.50 3.60 3.70 3.80 3.90 01 r > P . ! | > I । | . H................. 1 1 I 1 ' 1 ■ i 1 ■ ■ ■ i 1 1 m/ Z 81.90 54.99% n/z-> 10 20 30 40 50 60 90 70 100 80 110 Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 74 82

5000 4 3.50 3.60 3.70 3.80 3.90 1 1 ''•'T' 1 47 m/ z 83.95 38.82% 35 12 । 108 0 -H-PP - --- 1 MTrrr > । . > । i । । । miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 74 3.50 3.60 3.70 3.80 3.90 5000 82 m/z 76.00 30.88% 47 35 .........................'|,1 1 ,., ,11,,,, L . 109 0 I 1 ' I 1 I ' 1 ' TI1 1 1 I '“I ' 1 1 1 1 1 1 /z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11643: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... " I1 1 ' 'I'" 1 I" ‘ ‘ I ‘ ‘‘ I1 1 74 3.50 3.60 3.70 3.80 3.90 m/z 47.00 24.29% 47 82 5000

38 ........................... I , 95 102 108 0 ■ 1 i ■ ■ ■ ■ i ■ 1 ■ ' i ’ i ' ■ i ■ ■ ■ ■ i ■ ' ' ■ i ■ I 1 i ' ''' Irduoti r /z-> 10 20 30 40 50 60 70 80 90 100 110 3.50 3.60 3.70 3.80 3.90

30561.D SCAN508.M Wed Jan 16 08:14:13 2002 Page 3

NYC-WTC_000051761