Laboratory report listing unknown compounds and surrogate recovery for sample AE00250 analyzed on January 28, 2002.
NYC-WTC_000050596–000050614Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document uLaLy otatti totpounu Keporc
Data File : C:\MSDCHEM\1\5973N\02JAN24\00250.D Vial: 6 . Acq On : 24 Jan 2002 7:06 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 3-Buten-2-ol, 2-methyl- Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T. 5.02 0.30 ug/L 148217 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 80 2 3-Buten-2-ol, 2-methyl- (CAS) $$... 86 C5H10O 000115-18-4 80 3 Butenol, methyl- 86 C5H10O 060766-00-9 80 4 3-Buten-2-ol, 2-methyl-86 C5H10O 000115-18-4 64 Abundance Scan 144 (5.018 min): 00250.D (-) m/z 71.10 100.00% 43 71
5000
39 55 59
67 84 4 4.60 4.80 5.00 5.20 5.40 - HH ‘I ’" ’il'' ’i ’ ”' i m/z 43.10 91.95% m/z—> 5 10 15 20253035404550556065 70 75 808590 Abundance #4083:3-Buten-2-ol, 2-methyl- 7h 43 5000 59 I 1 ■ • ‘i • 4.60 4.80 -4 4A-A-2/4 5.0) 5.20 5.40 27 31 m/z 41.10 55.95% 53 >, ।.... । ।. 1111. ।. ■HT —3% .86 — ।.. j.... ।.... ।,,.. ।... > । mfz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #4081:3-Buten-2-ol, 2-methyl- (CAS) $$ 2-Methyl-3-buten-2... 71 4/), 4 43 4.60 4.80 5.00 5.20 5.40 5000- m/z 59.10 39.20% 59 27 31 53 67 nidmapaniri H mipl# t n/z-> 5 10 15 20 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #4093: Butenol, methyl- A..... A 1 1 ’ ‘ I * ‘ 1 ’ 1 * ‘ 43 7! 4.60 4.80 5.00 5.20 5.40 m/z 69.10 34.81%
5000 59 27 15 31 53 ’ ’’11117 “ ■■1111 ‘i ‘ ’II -H 67,• 11 , I“। >j• I 86 A, A mfz~> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 4.60 4.80 5.00 5.20 5.40
0250.D SCAN508.M Fri Jan 25 10:26:23 2002 Page 7
NYC-WTC_000050606
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NYC-WTC_000050481
Laboratory report for sample AE00167 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051967
GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050539
Laboratory report for sample AE00247 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050519
Laboratory report for sample AE00169 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051842
Gas chromatography-mass spectrometry analysis of sample AE00703 conducted on 1/28/02, detecting unknown compounds and 2,4-DDD surrogate at 117 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051930
GCMS analysis log for sample AE00737 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050645
Laboratory report listing unknown compounds and surrogate recovery for sample AE00110 analyzed on February 13, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051549
Laboratory report showing GCMS analysis results for sample AE00556 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050754
Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050735
Laboratory report listing unknown compounds and surrogate recovery for sample AE00027 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051586
Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006126
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03247 conducted on March 15, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050432
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050433
Fragmented page containing a document identifier and instructions regarding liquid-liquid extractor drip rates from January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050435
Gas chromatography-mass spectrometry calibration analysis of sample AE00167 detecting multiple organic compounds including nitrosamines and dichlorobenzenes.
Filed in the same folder
NYC-WTC_000050439
Laboratory report listing concentrations of volatile organic compounds in sample AE00167 analyzed on January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050444
Laboratory blank report for GCMS analysis of sample AE00167 showing compound concentrations and quality control values.
Filed in the same folder