GCMS data file header for sample AE00700, Jan 16 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN16\00700.D Vial: 5 Acq On : 16 Jan 2002 2:11 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 Docosa-2,6,10,14,18-pentaen... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 33.59 0.23 ug/L 120586 Perylene-dl2 34.42 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Docosa-2,6,10,14,18-pentaen-22-a... 384 C27H440 000000-00-0 86 JO 2 10-DEMETHYLSQUALENE $$ 2,6,10,14... 396 C29H48 059681-06-0 86 009 3 Squalene 410 C30H50 007683-64-9 80to 4 2,6,10,14,18,22-Tetracosahexaene... 410 C30H50 000111-02-4 72 Abundance 63 Scan 2647 (33.594 min): 00700.D (-) m/z 69.10 100.00%

5000 41 ■ ■ i ■ ■

93 119137 0- — +444 TT 207 I ■" i I" •' I ” " 11"1111111 33.20 33.40 33.60 33.80 34.00 m/z 81.10 51.99% n/z-> 40 60 80 100 120 140 160180 200 220 240 260 280 300 320 340 360 380 400 _ Abundance #323104: Docosa-2,6,10,14,18-pentaen-22-al, 2,6,10,15,18-p... 69

5000 33.20 33.40 33.60 33.80 34.00 93 m/z 41.10 24.54% 111 136

m/z-> 0 i" " i Abundance I , I ill .II I 161 192................ 273....... 315...... 357 384....... 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 #330384:10-DEMETHYLSQUALENE $$ 2,6.10,14,18,22-Tetracosah... MMWANA 69 33.20 33.40 33.60 33.80 34.00 5000 m/z 68.10 14.18%

95 12 _ 0 ....... | . । । . . > ■ | iT। । ri .... 177... 223......267 । i V. i p i i T | r. i 11 i . . r । i i I i । । । । । 11 i i i 11 ■ 11 । n i i । 327 369 396 ■ i " " r'" ■ i' " ' i' ■" i" '' i" " i w n/z-> 40 60 80 100 120 140160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #337959: Squalene 69 33.20 33.40 33.60 33.80 34.00 m/ Z 67.10 14.00%

5000

95 137 0 111" ■1 r T‘0‘TTAETI-1119 J.. — -EEITT 368 191410 ■ i ' 1 ■ 1 । ■ > m/z-> 40 60 80 100 120140 160 180 200 220 240 260 280 300 320 340 360 380 400 33.20 33.40 33.60 33.80 34.00

)0700.D SCAN508.M Thu Jan 17 08:17:10 2002 Page 8

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