DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004935–000005145

Folder label: “GCMS X 2/1/02 A 2/27/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

. Data File : C:\MSDCHEM\1\5973N\02FEB27\02456.D Vial: 7 Acq On : 27 Feb 2002 8:18 pm Operator: Sample : 508 scan Inst : Instrumen Mise 2002 : February 27, Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 1,2-Benzenedicarboxylic aci... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.10 0.15 ug/L 101996 Chrysene-dl2 30.49

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, 3-... 211 C8H5NO6 000603-11-2 78 2 1,2-Benzenedicarboxylic acid, di... 390 C24H3804 000117-84-0 53 3 1,2-Benzenedicarboxylic acid, di... 390 C24H3804 027554-26-3 53 4 (IS*,2R*,5R*,7S*)-2,4-Dimethyl-7... 168 C10H16O2 091926-28-2 50 Abundance Scan 2456 (31.099 min): 02456.D (-) m/z 149.00 100.00% 149

5000 57 167 84 113 30.80 31.00 31.20 31.40 207 240 0 HA 4 TTTTITTTTNTTTTTTTTLTTTTTTTTTICWTTTTTTTTTTTTT 1111111 ■111 r m/z 57.10 35.97% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #131213:1,2-Benzenedicarboxylic acid, 3-nitro- (CAS) $$ 3... 149

----- 5000 30.80 31.00 31.20 31.40 167 m/z 167.00 29.13% 71 1 113.39 - 0- ‘ ‘ 4’111171111’1111 1’10-1—111111TTT"77111113T n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #326898:1,2-Benzenedicarboxylic acid, dioctyl ester (CAS)... 149 1 ' i ■ 30.80 31.00 31.20 31.40 5000 m/z 43.10 20.25% 57 167

m/z-> o1 LL 40 60 390 i111 ■ i' ” 11111111" 1111111 ■11 ■ i ■ " 1111" i " 11 [ " 11 r 11' i11" i11111 ■ " 11 ■ " 11 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #326922:1,2-Benzenedicarboxylic acid, diisooctyl ester (C... 149 30.80 31.00 31.20 31.40 m/ Z 71.00 19.41%

5000 57 167

/z-> J 0 1 ■i'1" i‘111111 “ r V111" 1111" 1111" i “ 11111" 111■‘11 ■" i111 ■ i " 1 ‘ i11" i “ 1 ■ i1 **11 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 390 "i""i ■ ■ । । > 1 ■ 30.80 31.00 31.20 31.40 ' ' i 1 ' 1 1 i ' '

02456.D HP022102.M Thu Feb 28 08:47:50 2002 Page 15

NYC-WTC_000005144

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NYC-WTC_000005144Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999