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GCMS analysis results for sample AE01638, March 2002

Machine-extracted title · confidence 100%

GCMS laboratory results for sample AE01638 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010126–000010145

Folder label: “GCMS X 1/23/02 A 2/21/02

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NYC 9/11 Public Portal Document Library Search Compound Report . - Data File : C:\MSDCHEM\1\5973N\02FEB21\01638.D Vial: 7 Acq On : 21 Feb 2002 8:11 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 1,2-Benzenedicarboxylic aci... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 31.10 0.05 ug/L 33561 Chrysene-dl2 30.49 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,2-Benzenedicarboxylic acid, di... 390 C24H3804 027554-26-3 23 2 1,2-Benzenedicarboxylic acid, di... 390 C24H3804 000117-84-0 9 3 2-((Trimethylsilyl)methyl)-3-((d... 222 C12H22N2Si 083781-66-2 5 4 4-Pyridinecarboxaldehyde, 3-hydr... 167 C8H9NO3 000066-72-8 5 Abundance Scan 2456 (31.099 min): 01638.D (-) m/z 149.00 100.00% 149

5000 57 167 226 207 ' 30.80 31.00 31.20 31.40 0- m/z 57.10 30.39% nz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #326922:1,2-Benzenedicarboxylic acid, diisooctyl ester (C... 149

5000 57 30.80 31.00 31.20 31.40 167 m/z 167.00 27.01% 0- ... ... ... 11.................. 390 niz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #326898:1,2-Benzenedicarboxylic acid, dioctyl ester (CAS)... 149 ■ 1 i ■ 1 ■ ■ i T 30.80 31.00 31.20 31.40 5000i m/z 49.00 26.74% 57 167 A 1 1 390 0 1111110021—t9—*"12100001m*9uuuauuuuona—d n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #147362:2-((Trimethylsilyl)methyl)-3-((dimethylamino)meth... 73 149 30.80 31.00 31.20 31.40 179 207 m/z 70.00 25.62% 5000 106

0- • • i • ■ • * i' *' • i • ■ • • i ■ * ■ ■ i • > * * i • * ■ • i i.. 11 Ju ? 2 T T m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 30.80 31.00 31.20 31.40

01638.D HP022102.M Mon Feb 25 10:55:52 2002 Page 15

NYC-WTC_000010144

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NYC-WTC_000010144Source: NYC Law Department, mirrored locally

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