DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report

. Data File : C:\MSDCHEM\1\5973N\02FEB27\02456.D Vial: 7 Acq On : 27 Feb 2002 8:18 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 12 Phenanthrene-dlO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.48 ug/L 342767 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-dlO 188 C14D10 001517-22-2 72 2 N(1), N(2)-bis[(Furan-2-yl)methy... 188 C10H8N2O2 000000-00-0 50 3 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 47 4 anti-10-hydroxy-5,6,8,9-tetrahyd... 188 C12H1202 055139-53-2 43 Abundance Scan 1718 (22.768 min): 02456. D (-) m/z 188.10 100.00% 188

5000 ............ ....... ................................. 94 80 22.40 22.60 22.80 23.00

mfe-> 0 11 । । TT TH 52 *1 < ।'1।11 66 IIT 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 132 146 158 180, L m/ z 94.00 21.13% Abundance #84499: Phenanthrene-d 10 188

5000 ■ । ' ■ ■ 1 i 1 11tt , . . . । . , . , [ . 22.40 22.60 22.80 23.00 m/z 189.10 16.41% 80 94 160 66

miz—> 0 30 i ■ ■1 ■ i11 r 111'1 ■ i'1' ■ i ■ ■

40 50 60 70 80 dl..... ........ 90 100 110 120 130 140 150 160 170 180 190 Abundance #97589: N(1), N(2)-bis[(Furan-2-yl)methylene]hydrazine 52 188

39 22.40 22.60 22.80 23.00 5000 m/ z 80.00 12.76% 80 94 103 131 66 | 160 0 11111! 111 ■ ■ I ‘ II TI ITT m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-dlO ■ i ■ 1 PT............ ’ ' i ' 188 22.40 22.60 22.80 23.00 m/z 184.10 9.87%

5000

80 94 66 158 0'| 11,, ।, rrp ,, ।, HT TTt —LPmTHP 7 mfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00

02456.D HP022102.M Thu Feb 28 08:47:50 2002 Page 14

NYC-WTC_000005143