GCMS DFTPP calibration report, Feb 5 2002

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Library Search Compound. Report Data File : C:\MSDCHEM\1\5973N\02FEB05\00003A.D Vial: 2 Acq On 5 Feb 2002 3:46 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 p-Terphenyl-dl4 Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 29.68 0.04 ug/L 51671 Chrysene-dl2 30.51 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 p-Terphenyl-dl4 244 C18D14 001718-51-0 53 2 6-methyl-5-(3 4‘-methylenedioxy... 244 C12H12N402 000000-00-0 50 3 Sophoramine 244 C15H20N2O 006882-66-2 45 4 1-Pyrenecarboxaldehyde hydrazone 244 C17H12N2 076465-53-7 45 Abundance Scan 2304 (29.678 min): 00003A.D (-) m/z 244.10 100.00% 244

6000

' ' 1 1 ■ 49 - 84 122 207 . 29.40 29.60 29.80 30.00 ■ i ■ ■

0-I m/Z 243.10 52.23% iz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #160355: p-Terphenyl-d14 244

5000 29.40 29.60 29.80 30.00 m/z 122.00 16.45% 122 106 160 184 198 212 226 01 ■ i i | i ■ ■ i > ■ 1itF bi 1 . | Z—> 40 60 80 100 120 140 160 180 200 220 240 Abundance #178493: 6-methyl-5-(3‘,4‘-methylenedioxypheny!)pyrimidine... 2414

29.40 29.60 29.80 30.00 5000 m/z 242.10 14.61%

185 0--- miz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #179289: Sophoramine 24 4 29.40 29.60 29.80 30.00 136 m/z 245.00 13.45% 5000 149 215 96 109 122 160 172 OTT ....... 7 I ,I, I 186 — ' i 1 1 1 1 1 ' ' ' I ................ • ' I 1 1 1 ‘ I ' ' 1 I ' 1 1 ' i ' 1 m/z—> 40 60 80 100 120 140 160 180 200 220 240 29.40 29.60 29.80 30.00

00003A.D SCAN508.M Thu Feb 21 10:18:51 2002 Page 15

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