GCMS DFTPP calibration report, Feb 5 2002

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Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB05\00003A.D Vial: 2 Acq On 5 Feb 2002 3:46 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ************* ******************************************************** Peak Number 12 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.37 ug/L 437426 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual I DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 91 2 Anthracene-dlO- 188 C14D10 001719-06-8 86 3 Acridine-D9 188 C13D9N 000000-00-0 64 4 2,2'-bipyridine-N,N'-dioxide 188 C10H8N2O2 000000-00-0 59 Abundance Scan 1699 (22.771 min): 00003A.D (-) m/z 188.15 100.00% 188

5000

94 80 160 22.40 22.60 22.80 23.00 23.20 42 52 64 118 136 146 . । 1801J 0- T........ . ’ l ' । । ' (r. ■ । tylir 11* th ■ ■1 • । ■ • ■ ■ | Ill’ll ■ ■ ■ n m/z94.10 15.84% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 22.40 22.60 22.80 23.00 23.20 80 94 m/z 189.10 12.88% 66 158 0- " i " " i1 " 11 ■ ■111 ■ TIT ■ > i > 111 ■ 11 ■ 11 ■ ।1 ■ ■ > l ■ >-< > l >1 • ■ i • > ■ ■ i ■ ■11’| ■ ■ ■ ■ i ■ "11'1111 ‘ ‘‘I m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- 188

22.40 22.60 22.80 23.00 23.20 5000 m/z 184.10 10.62%

94 160 , , 0- ■ 11 ■ ■ । ' 66 T । ■ ■ ■ ■ । 11 ■ । ■ ■ - -1 ■ 11111" I " ■11" " i" .........T... 189,.... miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #85254: Acridine-D9 188 22.40 22.60 22.80 23.00 23.20 m/z80.10 10.18%

5000

93 158

/z-> 0 66 " i ■■ ■ ■ i' " 'i■■'■ i " ■ &.L 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 TT —l 22.40 22.60 22.80 23.00 23.20

00003A.D SCAN508.M Thu Feb 21 10:18:51 2002 Page 14

NYC-WTC_000004817

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NYC-WTC_000004817Source: NYC Law Department, mirrored locally

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