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GCMS surrogate recovery results for sample AE00278, Jan 2002

Machine-extracted title · confidence 90%

Laboratory record documenting GCMS surrogate recovery data for sample AE00278 analyzed on January 10, 2002.

NYC-WTC_000050856–000050874

Folder label: “GCMS X 1/7/02 A 1/9/02

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Scanned page image, NYC-WTC_000050868
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN09\278.D Vial: 3 Acq On 9 Jan 2002 7:50 pm Operator: ■ Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 p-Terphenyl-dl4 Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

27.54 0.12 ug/L 109947 Chrysene-dl2 30.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 p-Terphenyl-dl4 244 C18D14 001718-51-0 72 2 1-Pyrenecarboxaldehyde hydrazone 244 C17H12N2 076465-53-7 64 3 5-HYDROXY-5,6-DIDEHYDROKAWAIN $$... 244 C14H1204 060037-36-7 60 4 1-phenyl-perimidine 244 C17H12N2 000000-00-0 59 Abundance Scan 2117 (27.543 min): 278.D (-) m/z 244.20 100.00% 244

5000

122 198 212 226 27.20 27.40 27.60 27.80 40 78 94 106 136 160 o1---------------------- 1 1 i ■ ■ 1 ' I ' ■ ■ ■ i 1 -PT—+ m/z 122.10 19.11% m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #160355: p-Terphenyl-d14 2414

5000 i1111 r1 11 1 i 1 27.20 27.40 27.60 27.80 m/z 245.20 17.00% _ 122 106 i 160 184 198 212 226 0 1 1—— TBTr ‘T ■ i l - nt T)/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #179479:1 -Pyrenecarboxaldehyde hydrazone 2414 v 27.20 27.40 27.60 27.80 5000 m/z 243.20 14.27% 201 122 228 100 213 I 01 ' ■ i ' 1 ■ ■ i 1 ' ' ■ i ■ ■ ' ' I ' — TTF m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #178835: 5-HYDR0XY-5,6-DIDEHYDR0KAWAIN $$ 2H-Pyran-2-one,... ■ ‘ I TTT’ 131 244 27.20 27.40 27.60 27.80 69 103 m/z 240.20 9.44%

5000 84

145156 173183 199 0-11/0/1/0/0/0/0) 47 . I r11 ■ ' i ' /z—> 40 60 80 100 120 140 160 180 200 220 240 27.20 27.40 27.60 27.80

278.D SCAN508.M Thu Jan 10 11:51:45 2002 Page 8

NYC-WTC_000050868

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NYC-WTC_000050868Source: NYC Law Department, mirrored locally

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