GCMS analysis results for sample AE00842, Feb 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00842 including surrogate recovery and unknown compounds.

NYC-WTC_000052251–000052270

Folder label: “GCMS X 1/11/02 A 2/7/02”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Data File : C:\MSDCHEM\l\5973N\02FEB07\00842.D Vial: 6 Acq On : 7 Feb 2002 6:34 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.68 ug/L 451044 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 86 2 anti-10-hydroxy-5,6,8,9-tetrahyd... 188 C12H1202 055139-53-2 58 3 2,2,9,9-Tetramethyldec-5-ene-3 ,7... 188 C14H20 102745-35-7 47 4 Anthracene-diO-___________________ 188 C14D10 001719-06-8 42 Abundance Scan 1699 (22.771 min): 00842.D (-) m/z 188.10 100.00% 188 N

5000

94 TT 11 22.40 22.60 22.80 23.00 23.20 l ' ' ■ ■ i ■

122 158 m/z-> 42 54 64 0- ■ ■ ■ |l.. ■ l ll ■ 78 ■ I .... ..... I i'' ■ ■ i 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 132+146,4 ........1' tr m/z 94.10 19.43% Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 22.40 22.60 22.80 23.00 23.20 80 94 m/z 189.10 19.08%

m/z-> o1 11" " ।' 40 50 TP 66 1 ‘‘T 158 1111111111111111111111111'1 ■ ’ ■ ‘ 11' 60 70 80 90 100 110 120 130 140 150 160 170 180 190 —l Abundance #98076: anti-10-hydroxy-5,6,8,9-tetrahydro-5,9-methano-7H-... 128 188 115 ‘F TT 22.40 22.60 22.80 23.00 23.20 5000 145 m/z 184.10 9.22%

158

m/z-> 0- 40 I'''' I " '' Ik’ I' ‘ ‘U‘ 50 60 i " ' ■ i ■ " ■ i 70 80 90 100 110 120 130 140 150 160 170 180 190 I.. I..... i " ■ ■ i ............ ........................................ Abundance #98584: 2,2,9,9-T etramethyldec-5-ene-3,7-diyne 1(18 22.40 22.60 22.80 23.00 23.20 173 m/z 158.10 8.87% .. 131 143 ft 5000 77 158 119

—— i' ■'' r '' ■ i I '"I i ■ ■ • ■ i I.. TT / T TIT m-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

00842.D HP020702.M Thu Feb 21 09:58:10 2002 Page 13

NYC-WTC_000052267

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000052267Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

GCMS analysis results for sample AE00844, Feb 26 2002 · Box DEP Box 28

NYC-WTC_000052291

Laboratory report detailing GCMS scan results for sample AE00844, including detection of unknown compounds and surrogate recovery data.

1 shared topics · Same agency, volume and box · similarity 0.999