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GCMS surrogate recovery results for sample AE00279, Jan 2002

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Laboratory record documenting GCMS surrogate recovery data for sample AE00279 analyzed on January 10, 2002.

NYC-WTC_000050875–000050892

Folder label: “GCMS X 1/7/02 A 1/9/02

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Scanned page image, NYC-WTC_000050890
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NYC 9/11 Public Portal Document Jisicay ‘ L

Data File : C: \MSDCHEM\1\5973N\02JAN09\279.D Vial: 4 Acq On 9 Jan 2002 8:40 pm Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.28 ug/L 226799 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual I DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 90 2 Anthracene-dlO- 188 C14D10 001719-06-8 80 3 anti-10-hydroxy-5,6,8,9-tetrahyd... 188 C12H1202 055139-53-2 53 4 2,2,9,9-Tetramethyldec-5-ene-3,7...188 C14H20 102745-35-7 50 Abundance Scan 1699 (22.771 min): 279.D (-) m/z 188.10 100.00% US

5000 -------------------I--------- 80 94 22.40 22.60 22.80 23.00 23.20

n/z-> 0 42 52 66 "i""i"111 ruisiml. ■ ‘ ।1 ■ i " 1' i1 • i ■ ■ •11 Ae 158 ......... I ITT 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 L m/z 189.15 16.56% Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenantbrene-d10 188

5000 22.40 22.60 22.80 23.00 23.20 80 94 m/z94.00 16.44%

n/z-> 0 ■ । 66 i ■■■■i■ ■1 ■ i■ ■1 '•'1111T7 । 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ■1 ■ । J ।■11 158 ।1111'|1111111 l Abundance #84502: Anthracene-d10- US ,1111 P) , , , — 22.40 22.60 22.80 23.00 23.20 5000 m/z80.00 11.56%

■n/z-> 0- .21 ..... T... 1894 i • • ■ ■ i • ■ ■ ■ i 40 50 . 60 70 80 90 100 110 120 130 140 150 160 170 180 190 160 .| T-m-r

Abundance #98076: anti-10-hydroxy-5,6,8,9-tetrahydro-5,9-methano-7H-... f | I I ! I 1 1-1 1~|-1 "I I I ) . . . . ( I

128 KS 22.40 22.60 22.80 23.00 23.20 115 m/z 184.10 7.99%

5000 145

158 ।" " i ■■1 ■ । i■■ ■■ i । ■■ ■ ■ । .......... . .............. — m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

279.D SCAN508.M Thu Jan 10 11:51:50 2002 Page 11

NYC-WTC_000050890

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NYC-WTC_000050890Source: NYC Law Department, mirrored locally

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