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GCMS surrogate recovery results for sample AE00279, Jan 2002

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Laboratory record documenting GCMS surrogate recovery data for sample AE00279 analyzed on January 10, 2002.

NYC-WTC_000050875–000050892

Folder label: “GCMS X 1/7/02 A 1/9/02

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Scanned page image, NYC-WTC_000050889
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\O2 JANO9\279.D Vial: 4 Acq On : 9 Jan 2002 8:40 pm Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

22.28 0.14 ug/L 115453 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 64 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 58 3 Anthracene, 1-methyl- 192 C15H12 000610-48-0 50 4 2-CYANOCARBAZOLE $$ 9H-Carbazole... 192 C13H8N2 057955-18-7 50 Abundance Scan 1656 (22.280 min): 279.D (-) m/z 192.10 100.00% 19 2

5000

96 TiB 82 40 66 | 118 146 160 11 22.00 22.20 22.40 22.60 0 —PH । ■ 11 >111•1111*11'h" ।< ...I.... -TIT m/z 193.10 17.65% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424: 3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192

5000 22.00 22.20 22.40 22.60 96 164 m/z 96.00 17.52%

m/z-> 0 I •» " I••••i " r • । । mmmm L 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 TTTT 138 X Abundance #88409: N-perdeuteriobenzylideneaniline 192

22.00 22.20 22.40 22.60 5000 82 m/z 191.00 16.55%

54 110

m/z--> 0 30 — I' ‘ "T i■■ • • i ■ i 94 .. ... -.. I...... 1 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 160 4 Abundance #103908: Anthracene, 1-methyl- TT 192 22.00 22.20 22.40 22.60 m/Z 146.10 15.33%

5000

82 94 165 0 I II 152 , 176 , ........ . ...... .. ................. 1...... 11............ ..................... ........................... . TTp- _A 1 1 ' ' 1 r i n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

279.D SCAN508.M Thu Jan 10 11:51:50 2002 Page 10

NYC-WTC_000050889

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NYC-WTC_000050889Source: NYC Law Department, mirrored locally

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