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GCMS results for sample AE00471, Jan 18 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00471 with surrogate recovery data on January 18, 2002.

NYC-WTC_000051301–000051317

Folder label: “GCMS X 1/8/02 A 1/10/02

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Scanned page image, NYC-WTC_000051316
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN10\00471.D Vial: 6 Acq On 10 Jan 2002 6:57 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 10 Phenol, 2,4-bis(1-phenyleth... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

30.66 0.27 ug/L 143641 Chrysene-dl2 30.49

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenol, 2,4-bis(1-phenylethyl)- 302 C22H220 002769-94-0 94 2 (+-)-cis-3,4,6,9-tetrahydro-10-h... 302 C17H1805 124821-09-6 83 3 2,4-Di (1 -phenylethyl) phenol $$ P...302 C22H220 002769-94-0 64 4 3,3'-dideuterio-l-acetyl-2-(trim../ 302 C15H18D2FeOSi 134455-20-2 50 Abundance Scan 2390 (30.660 min): 00471 .D (-) m/z 287.20 100.00% 287

5000 302

105 209

49 77 91 । 136 152165 119 . h i . .. 181194 1. " , ,1,1, , ,1, , 30.40 30.60 30.80 31.00 47.55% i h i o rrorrtn) I 11 11I T m/z 302.20 n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #252672: Phenol, 2,4-bis(1-phenylethyl)- 287

302 5000 ’ I’* TT 1 1 1 । 1 ' . । i ■ ■ 30.40 30.60 30.80 31.00 105 136 209 m/z 209.10 27.48%

0' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ‘ ' ' I ' ' ■R .... TTT t r-r /z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #251932: (+-)-cis-3,4,6,9-tetrahydro-10-hydroxy-7-methoxy-... 287 /.A.... . 30.40 30.60 30.80 31.00 5000 m/z 288.20 25.97% 302

0^ 60 80 100 120 140 160 180 200 220 240 260 280 tT— /z- > 40 300 Abundance #252673:2,4-Di(1-phenylethyl)phenol $$ Phenol, 2,4-bis(1-... 287 30.40 30.60 30.80 31.00 183 302 m/z 105.05 24.39%

5000 105 198

0 • ■ । • ■«' । ■ ■ > • । ■ ■ • ■ । ■ ■ < ■ । • TTUi -44 PAer iz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 30.40 30.60 30.80 31.00

00471.D SCAN508.M Fri Jan 11 10:08:50 2002 Page 12

NYC-WTC_000051316

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NYC-WTC_000051316Source: NYC Law Department, mirrored locally

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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machine-extracted · confidence unavailable · Check page ↗

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