GCMS analysis report for sample AE01509, March 2002

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GCMS laboratory results for sample AE01509 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010008–000010026

Folder label: “GCMS X 1/23/02 A 2/21/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report ' Data File : C:\MSDCHEM\1\5973N\02FEB21\01509.D Vial: 1 Acq On : 21 Feb 2002 3:10 pm Operator: Sample : 508 scan Inst ■ : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Dibutyl phthalate $$ 1,2-Be... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 24.86 0.07 ug/L 51397 Phenant hrene-d10 22.64 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Dibutyl phthalate $$ 1,2-Benzene... 278 C16H2204 000084-74-2 83 2 Dibutyl phthalate 278 C16H2204 000084-74-2 83 3 1,2-Benzenedicarboxylic acid, bu... 334 C20H30O4 000084-78-6 83 4 1,2-Benzenedicarboxylic acid, di... 278 C16H2204 000084-74-2 83 Abundance Scan 1903 (24.857 min): 01509.D (-) m/z 149.00 100.00% 149

5000

41 57 76 105 121 205 223 24.60 24.80 25.00 25.20 11 m/z 150.00 10.38% 0-—mTpmmmm-mmP miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223242: Dibutyl phthalate $$ 1,2-Benzenedicarboxylic acid... 149

5000 ■ 1 i ■ ■ ■ ■ i 24.60 24.80 25.00 25.20 m/z 41.10 7.41% 41 56 76 104 121 205 223 278 0 ---------------- ■ i ■ ■ ■ ■ i ■ ‘ ■ i ■ 1

iz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223237: Dibutyl phthalate 149 ■ > j > • • > ] • • • i * • • ■ i ■ > 24.60 24.80 25.00 25.20 5000 m/z 76.00 4.79%

41 56 76 104 121 | ■ ■1 -r 11', . । । i11 1111 11 205 223 278 0 TIn 1 i 1 । । r j ( 11 ।. j 111 < । PmTrPi । n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #284876:1,2-Benzenedicarboxylic acid, butyl octyl ester 149 24.60 24.80 25.00 25.20 m/z 105.00 4.71%

5000

42 57 76 104 121 0' ‘ ‘ I * * ‘ I I ‘ ‘ * J 1 1 I » I I ‘ I ‘ i l I I ,1 .। । ,192295 223 . 261 279 iz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 24.60 24.80 25.00 25.20

01509.D HP022102.M Mon Feb 25 10:55:04 2002 Page 13

NYC-WTC_000010024

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NYC-WTC_000010024Source: NYC Law Department, mirrored locally

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