GCMS analysis results for sample AD31671, Jan 28 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02 JAN17 31671 .D Vial: 6 Acq On : 17 Jan 2002 6:59 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Phenanthrene-diO Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

22.77 0.30 ug/L 175698 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene-diO 188 C14D10 001517-22-2 91 2 Anthracene-dlO- 188 C14D10 001719-06-8 87 3 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 50 4 anti-10-hydroxy-5,6,8,9-tetrahyd... 188 C12H1202 055139-53-2 50 Abundance Scan 1699 (22.771 min): 31671 .D (-) m/z 188.10 100.00% 188

5000 ri i i 4. + r । i i । r ■ i i । i 80 94 132 158 22.40 22.60 22.80 23.00 23.20 0 +40,49. ffH,. 1. mTTTTT mz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 1’1 m/z 94.10 18.12% Abundance #84499: Phenanthrene-d10 188

5000 - —P m M । । । । । । i 22.40 22.60 22.80 23.00 23.20 80 m/z 189.20 17.68% 94 160 66 0 " 11' " 111111"'' I " 1 - ...................... [L.... ... 1 miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d1 0- 188

22.40 22.60 22.80 23.00 23.20 5000 m/z 80.10 14.63%

80 94 160 66 - Of “ । * * * * ।» 1 ■11'11 ri111 mz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188 22.40 22.60 22.80 23.00 23.20 m/z 184.10 11.71%

5000

80 94 — 0 66 111 ■' ■ • i ■ “11" ।111111 — 114 A ■ i ■ ‘ • i ■ niz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

31671.D SCAN508.M Tue Jan 22 08:37:27 2002 Page 10

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