GCMS analysis results, sample AE02718, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB28\02718.D Vial: 3 Acq On : 28 Feb 2002 4:20 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 50.8 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.

22.28 0.11 ug/L 70950 Phenanthrene-diO 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64 3 Benzo[1,2-c:3,4-c]bis(isothiazol... 192 C8H4N2S2 074960-05-7 53 4 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 50 Abundance Scan 1675 (22.283 min): 02718.D (-) m/z 192.00 100.00% 1512

5000

2 66 82 96 146160 22.00 22.20 22.40 22.60 0 - i-rp-r m/z 191.00 19.21% m/z—> 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588:4-METHOXY-BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 5000 1 !I4t 1" ri 22.00 22.20 22.40 22.60 146 175 m/z 146.10 14.23% 0 ‘‘ I “ “ I *1 ‘ ’ I" “ f ‘1 “ I “ “ I “ “ I ‘ ‘1 ‘ I ‘ ‘ ‘ 11*2330117 Hang M-rr m/z—> 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192 .......... A....... I ‘ 1 I ‘ ‘ ■ i ‘ ‘ 1 ' I 1 ' 1 ' 1 1 1 1 22.00 22.20 22.40 22.60 5000 82 m/z 193.00 12.29% 54 110 30 m/z—> 0 ungamnap mHm i TTIWTITTTTTT 94 160 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102104: Benzo{1,2-c:3,4-c]bis(isothiazole)$$ Benzo[1,2-c... 192 22.00 22.20 22.40 22.60 m/z 96.10 11.11% L

5000 45 148 57 69 82 96 121 165 1. i‘‘.1. 0 • ।111'i"■• I.__ 0__ L I ..pil.p.niTi.ip ***1‘‘‘‘2*8* ■i “111 ■ ■ ■ ■ i mmmm T‘‘r m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

02718.D HP022102.M Fri Mar 01 10:07:29 2002 Page 13

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