DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000003981–000004147

Folder label: “GCMS X 1/29/02 A 2/1/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\5973N\02FEB01\0129B.D Vial: 1 Acq On : 1 Feb 2002 10:35 am Operator: Sample : lab blank 1/29 Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L Peak Number 12 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.13 ug/L 90201 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 59 3 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 53 4 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 Abundance Scan 1656 (22.280 min): 0129B.D (-) m/z 192.10 100.00% 192

5000

1 1 i ' 1 1 1 I ------- 82 96 146 160 70 22.00 22.20 22.40 22.60

n/z-> 49 0 " i ■ ■' ■ i ‘ — 40 /..... 118..... 111 — -p 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 rn/z 191.10 14.94% Abundance #102588: 4-METHOXY-BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 102

108 5000 22.00 22.20 22.40 22.60 146 175 m/ z 146.10 14.35%

0 1‘11111111111111111071110T10111IT0T i'' " i11 " i' " ' r ' ' । ■ * 111 11 1 * । ■ .. "I1 11’3 m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102099: Thiocyanic acid, 2-benzothiazolyl ester $$ 2-Benz... 192 A* 22.00 22.20 22.40 22.60 5000 m/z 193.10 12.63%

45..... 1 66 82 90 108 122; 114 148 160 o1 " I'1 " 11 " ' I ‘-—— H m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103930: Phenanthrene, 2-methyl- 192 22.00 22.20 22.40 22.60 m/z 96.00 11.59%

5000

96 139 152 165 176 0 ........................................ . ................ ‘I' ■1' 111'11 ‘11' I' 11 ■ i ■ ■ " i ■ ■ ■ ■ i'1' '11'111111 ■ i ’I’ > । >' i > 11 TT m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

0129B.D SCAN508.M Mon Feb 04 08:40:59 2002 Page 14

NYC-WTC_000004008

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999