DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document library search compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB27\02453.D Vial: 4 ’ Acq On : 27 Feb 2002 5:47 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 N-(2-methylprop-2-enyl)-2-n... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.12 ug/L 77838 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-(2-methylprop-2-enyl)-2-nitrob. .. 192 C10H12N2O2 000000-00-0 43 2 fluorene-9-spiro-cyclopropane 192 C15H12 000000-00-0 42 3 2-CYANOCARBAZOLE $$ 9H-Carbazole... 192 C13H8N2 057955-18-7 42 4 1-(2-THIENYL)-2-(3-THIENYL)ETHENE 192 C10H8S2 087441-44-9 40 Abundance Scan 1675 (22.283 min): 02453.D (-) m/z 192.00 100.00% 192

5000

146 ________ , ■ ■ i ■ ' r1,*111L’I1I 44 82 96 70 ■ ■ 111 ■ ■ t ■ H11111. > [i ■'' ।■ 111111 ■ । >. 160 . 22.00 22.20 22.40 22.60 Ot 1 ‘ I 1 1 '1 I' '1 ‘ 11 ' 1 1 I ‘ ' .... ..................... P m/z 146.10 19.06% II" n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine 192 77 151 130 93 104 5000 119 22,00 22.20 22.40 22.60 m/Z 193.10 18.43% 177 0 ■■i■■■■। . .. .... T-p-r ... ।11।' 'i । > ■ > ■ । 1IIT IIr TIIT i11 ■11 ■1111 ■ ■ ■ ■1111 ■ ■ i11 ■ ■ i

mfe-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103959: fluorene-9-spiro-cycIopropane 192

165 22.00 22.20 22.40 22.60 5000 m/z 191.00 16.41%

m/z-> ...... ....... 139.152 .. 0 111 n ' ■ i *1111 ■ ■1111 ■1111111 r 11 ■ i ■ ■ ■11 ■11 ■ i ■ ■111'1 ■ TTmtuu । "tt j 1111 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 11117

Abundance #103420: 2-CYANOCARBAZOLE $$ 9H-Carbazole-2-carbonitrile (CAS 192 22.00 22.20 22.40 22.60 m/z 96.10 14.31%

5000

164 96 138 iz—> 0 ' ■ i1' " i' " 11'111 r'' " I' " 1111'11 " 1111 rr r 11 " > । > 111'[ ।' । TTI 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 mm T-r-p-r-r-r-p- 22.00 22.20 22.40 22.60 TIT

32453.D HP022102.M Thu Feb 28 08:47:23 2002 Page 12

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