DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004935–000005145

Folder label: “GCMS X 2/1/02 A 2/27/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB27\02453.D Vial: 4 Acq On : 27 Feb 2002 5:47 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L Peak Number 9 3-Methoxybut-1-ene Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 19.98 0.02 ug/L 14413 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Methoxybut-1-ene 86 C5H10O 017351-24-5 7 2 2-CARBAMOYL-3-HYDROXY-4,5,5-TRIM... 186 C8H14N2O3 072700-98-2 7 3 Methyl 1-Methyl-2-propenyl Ether 86 C5H10O 000000-00-0 7 4 2-Buten-l-ol, 3-methyl- (CAS) $$... 86 C5H10O 000556-82-1 7 Abundance Scan 1471 (19.980 min): 02453. D (-) m/z 71.00 100.00% 71 186 43 5000 51 86 ■ । 1 r 1 ' । ■ 1 19.60 19.80 20.00 20.20 20.40 O*PTIPTLTTTT 1111’1110171111-1111101V1IU —1""TEITICTTD’III’T TI’ m/z 186.10 70.16% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #4108: 3-Methoxybut-1 -ene 71

55 43 5000 ’11/11 TTT । । । । । । 86 19.60 19.80 20.00 20.20 20.40 27 m/ Z 43.00 57.29%

miz-> . .. 1 0- ' I'1111 " 11111'1 [1 H 111001110111117001101111111010111’0110111111021117 :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #94657: 2-CARBAMOYL-3-HYDROXY-4,5,5-TRIMETHYL-1 -PYRROLINE ... 71 1 i ' ■ ■ 1 । ■ ' ' ■ i ■ ■ ' 1 i ■ 19.60 19.80 20.00 20.20 20.40 5000 55 116 m/z 51.00 39.22% 41 186 86 142

0-’I’ •" I " " I' " [11 111111 TrUI 11 1 [ " 1' 111 H I 111111' i1" 11'11 ■ i ■n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance■ #4190: Methyl 1-Methyl-2-propenyl Ether 7|1 19.60 19.80 20.00 20.20 20.40 m/z 185.00 36.48% 55 43 5000 86 27

0 11' " 1 r '111 1 ■ i1 H 1 । ' 1 ■ 1 । 1 ‘ i ■ ' 1 ' i ' ■ ■ ■ i ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 19.60 19.80 20.00 20.20 20.40

32453.D HP022102.M Thu Feb 28 08:47:23 2002 Page 11

NYC-WTC_000005080

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999