GCMS results for sample AE00329, Jan 24 2002

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Laboratory report showing GCMS analysis of sample AE00329 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051485–000051499

Folder label: “GCMS X 1/8/02 A 1/11/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN11\00329.D Vial: 3 Acq On : 11 Jan 2002 3:46 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 73628 Phenanthrene -dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Cyanocarbazole $$ 9H-Carbazole ... 192 C13H8N2 057102-93-9 64 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 58 3 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 52 4 2-CYANOCARBAZOLE $$ 9H-Carbazole... 192 C13H8N2 057955-18-7 50 Abundance Scan 1656 (22,280 min): 00329.D (-) m/z 192.10 100.00% 192

5000

96 146 160 82

/z—> o " । ■" ■ । ‘ 49 66 " i *n 11"1 ■ ।1 ■ ■. । h. ■ i. 11,i ■. 11 118 TWWPu, 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ll— 22.00 22.20 22.40 22.60 m/z 96.00 18.50% Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192

5000 22.00 22.20 22.40 22.60 96 164 m/z 191.10 16.09% 138 0 " I "1' i11" I " " I" " i ■ " ■ i1" ■ i ■ ■ 1 r ' ‘' i''111" " 111' । r ■ " i' " ' r ........... I Tpn mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192

22.00 22.20 22.40 22.60 5000: 82 m/z 193.10 15.95%

54 110 30 1 94 160 0 ITTTTTTTT " I" " i' ■ ......... ■ " i'1" i1' " r ' " i " '' I'' I’"......... I' TT •n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine ................. 192 22.00 22.20 22.40 22.60 77 151 m/z 146.10 15.91% 130 93 104 5000 119

177 0 " i'''' i ‘ ' i " " i'" ' i" "I " " I ‘ IT TT I1 ‘ ’11'1111 I 1'' I " " l •' n-' . ......................... M /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

00329.D SCAN508.M Mon Jan 14 10:46:47 2002 Page 9

NYC-WTC_000051497

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GCMS results for sample AE00321, Jan 24 2002 · Box DEP Box 28

NYC-WTC_000051394

Laboratory report showing GCMS analysis of sample AE00321 with surrogate recovery data on January 24, 2002.

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