DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document Library searen compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB27\02453.D Vial: 4 ’ Acq On : 27 Feb 2002 5:47 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Phenanthrene-dlO Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.65 ug/L 432529 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

I Phenanthrene-dlO 188 C14D10 001517-22-2 59 2 N(l), N(2)-bis[(Furan-2-yl)methy... 188 C10H8N2O2 000000-00-0 50 3 Anthracene-D10 188 C14D10 000000-00-0 50 4 Anthracene-diO- 188 C14D10 001719-06-8 45 Abundance Scan 1718 (22.768 min): 02453. D (-) m/z 188.10 100.00% 188

5000 94 80 132 146 158 22.40 22.60 22.80 23.00 44 52 64 0m —----- ----- T। ’t m/z 94.00 26.09% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 188

5000 ...... / L .............. 22.40 22.60 22.80 23.00 m/z 158.05 12.60% 80 94 160 66 0 mTTTTT m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #97589: N(1), N(2)-bis[(Furan-2-yl)methylene]hydrazine 52 188

39 22.40 22.60 22.80 23.00 5000 m/ z 80.00 10.92% 80 94 103 131 66 I 160 mlz-> 0 i ■ ■' ■ i ‘'1' i 30 40 50 -HH 60 70 80 TTp- --mTmTPTTT 111 90 100 110 120 130 140 150 160 170 180 190 L Abundance #84498: Anthracene-D10 .......... / 1 I ' ' ‘ ' 1 1 • ■11 ■ ■ ■ ■ ।' 188 22.40 22.60 22.80 23.00 rn/z 160.10 10.27%

5000- 80 94 66 160

m/z-> mn ' 11 1111''' I'111111111''1111'1' 11' 111'11111'1' 11 ve TTuur 0 ।.... 11... 11।. 1. j.. 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00

32453.D HP022102.M Thu Feb 28 08:47:23 2002 Page 13

NYC-WTC_000005082