GCMS analysis results for sample AE01508, Mar 2002

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Analytical results for sample AE01508 analyzed via GCMS on March 4, 2002, including surrogate recovery data.

NYC-WTC_000009966–000009985

Folder label: “GCMS X 1/23/02 A 2/21/02”

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NYC 9/11 Public Portal Document Library Search Compound Report . Data File : C:\MSDCHEM\l\5973N\02FEB21\01507.D Vial: 4 Acq On : 21 Feb 2002 1:24 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ******************************************************************* * * Peak Number 6 2-Propanol, l,l'-oxybis- (C... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 9.61 0.05 ug/L 22138 1,4-Dichlorobenzene-d4 9.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, l,l'-oxybis- (CAS) $... 134 C6H1403 000110-98-5 9 2 2-Propanol, l,l'-oxybis- (CAS) $... 134 C6H1403 000110-98-5 9 3 2,3-Epoxy-3-methyl-6-methoxyheptane 158 C9H18O2 088083-53-8 9 4 2-Pentanol, 2-methyl- (CAS) $$ 2... 102 C6H140 000590-36-3 4 Abundance Scan 552 (9.605 min): 01507. D (-) m/z 59.00 100.00% 50

5000 45 73 103

86 9.20 9.40 9.60 9.80 10.00 0- * I *..H‘1 *‘1 1 ।J...।. . I.]....।J. । । । । । । . m/z 45.00 43.53% miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #29204:2-Propanol, 1,1‘-oxybis- (CAS) $$ Dipropylene glyc... 59

5000 31 45 ■ ■ i ■ ■ ■ ■ i ' ■

103 9.20 9.40 9.60 9,80 10,00 m/z 73.10 34.93% 01 • i • > • 113 > • • ।1... । • 4 1***s14*4t11*12214*8114*1*/11******1**** miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #29205:2-Propanol, 1,1-oxybis- (CAS) $$ Dipropylene glyc... 50 । , . , । , , , , MY , , / A , 31 9.20 9.40 9.60 9.80 10.00 5000 45 m/z 103.00 34.82% 103 N Z 0- •i■■■■i■■•■i *‘‘।।।1।।. 1 • ■ । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ i “ • ■ i ■ ■ ■ ■ i ■ ■ miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #57909:2,3-Epoxy-3-methyl-6-methoxyheptane 50 9.20 9.40 9.60 9.80 10.00 m/z 43.10 28.84% 5000 45 A 72 30 99 86 ... ..... II 126 143 01.1.... 1. '6144* . J. >.l. ». ] — ’ l * “ • I * ‘11 ’ ‘1 ‘ I ’ “ ’ I 158 * I' ‘'11 ’1 i ■ •11 I 111'r111 I' • ' i " m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 9.20 9.40 9.60 9.80 10.00

01507.D HP022102.M Mon Feb 25 10:54:51 2002 Page 8

NYC-WTC_000009977

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