GCMS results for sample AE00740, Jan 29 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

- Data File : C:\MSDCHEM\1\5973N\O2JAN16\00740.D vial: 8 Acq On : 16 Jan 2002 8:57 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 Pinacolyl alcohol Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

8.23 0.23 ug/L 90499 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm • CAS# Qual

1 Pinacolyl alcohol 102 C6H140 000464-07-3 38 2 Morpholine (CAS) $$ BASF 238 $$ ... 87 C4H9NO 000110-91-8 38 3 Morpholine $$ p-Isoxazine, tetra... 87 C4H9NO 000110-91-8 32 4 Morpholine (CAS) $$ BASF 238 $$ ... 87 C4H9NO 000110-91-8 12 Abundance Scan 425 (8.226 min): 00740.D (-) m/z 45.10 100.00% 45 57

5000 87

39 . 7.80 8.00 8.20 8.40 8.60

m/z-> 0 .. 10 ..... 20 30 J 40 '1' 50 1 ------- 60 70 80 — 90 ■ i • ■ 100 110 m/z 57.10 92.91% Abundance #9685: Pinacolyl alcohol 45 57

5000 l ‘ ■ i 69 87 7.80 8.00 8.20 8.40 8.60 m/z 87.00 42.78% 33 1 ' i ' 1 102 0- i ■ ' ■ ■ i • ' ' ' i ■ ■ 1m I ■ I > ■ 1 1' I > ■ > > I ' III m/z-> 10 20 30 40 50 60 90 70 100 110 80 Abundance #4372: Morpholine (CAS) $$ BASF 238 $$ Diethylene oximide... 29 57 7.80 8.00 8.20 8.40 8.60 5000 m/z 41.10 39.01% 87 15 42 - 0- —. — ' i ■ ■ ■ ■ । 1 1 1 1 । I1 I"'1 1I •■• •l /z-> 10 20 30 40 50 60 70 80 90 100 110 -- Abundance #4374: Morpholine $$ p-Isoxazine, tetrahydro- $$ BASF 238... - 23 57 7.80 8.00 8.20 8.40 8.60 m/z 56.10 30.13%

5000 87

42

m/z-> 0 10 20 30 n~i 40 52L I60'....... 50 70 I' 80 +TT 90 100 110 7.80 8.00 8.20 8.40 8.60

00740.D SCAN508.M Thu Jan 17 08:17:58 2002 Page 7

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