DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02FEB26\02017.D Vial: 5 Acq On : 26 Feb 2002 1:41 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 6, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 10 Methenamine Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 16.55 0.03 ug/L 21774 Acenaphthene-dl0 18.34 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Methenamine 140 C6H12N4 000100-97-0 7 2 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 7 3 1,3;5,7-Tetraazatricyclo[3.3.1.1... 140 C6H12N4 000100-97-0 7 4 Methylphloroglucinol 140 C7H803 000000-00-0 5 Abundance Scan 1167 (16.548 min): 02017. D (-) m/z 140.10 100.00% 140

5000

122 172 43 56 71 86 16.20 16.40 16.60 16.80 — 0- 1 ■ i ■1" i'1 ■ ■ i ■ 111" ■ i ■ — I " i" " r " ' i1" 11'" 11' m/z 172.20 28.87% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35197: Methenamine 42

5000 16.20 16.40 16.60 16.80 140 m/z 138.10 27.39%

niz-> OTT 15.27 71 85 112 1'' i1" ' r '1' Y' ■ ■ ■ i,''1' 111 111 " ■ 11 ■ ■ 11 u ., 11 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 11111 “ ।1 ■ ■11 ■ ■ ■111

Abundance #35040: Pyrimidinetetramine- $$ Pyrimidine, 2,4,5,6-tetraa... 140

16.20 16.40 16.60 16.80 5000 m/z 122.10 24.20%

44 71 123 86 96 112 0- -HH 111'1" ।'11''' ■ J ■111" T-p-r I.......................... I1' " i " " i " " r " 111 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35204:1,3,5,7-Tetraazatricyclo[3.3.1.1(3,7)]decane (CAS)... 42 16.20 16.40 16.60 16.80 m/ z 43.00 18.02%

5000 N 140 61 71 85 112 1’a -1 >" 111" । 'Y‘ 11' 111' ।' 11' 111'' 111111111111' i ""i ।'"I ""i '' I'11111''' 111'' 11 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 16.20 16.40 16.60 16.80

02017.D HP022102.M Wed Feb 27 08:34:40 2002 Page 12

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