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GCMS sample AE07115 results, April 25, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis results for sample AE07115 including detection of unknown compounds.

NYC-WTC_000049063–000049101

Folder label: “GCMS X 4/12/02 A 4/23/02

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Scanned page image, NYC-WTC_000049084
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\0410 02\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohik Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 4 1-Octadecene (CAS) $$ .alph... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

26.06 29.33 ug/L 4500250 Phenanthrene- dl 0 22.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Octadecene (CAS) $$ .alpha.-Oc... 252 C18H36 000112-88-9 97 2 1-Heptadecanol $$ n-Heptadecanol ... 256 C17H360 001454-85-9 95 3 5-Eicosene, (E)- 280 C20H40 074685-30-6 94 4 9-Eicosene, (E) -________________________ 280 C20H40 074685-29-3 94 Abundance Scan 3911 (26.059 min): 7115.D (-) m/z 55.10 100.00% 55 83

5000 111

25.80 26'00 26.20 26.40 m/z-> Of pmotha 1’1 4 » I ,’ J.,, 126 ,154 181196 .. 224 .. 252....... 1’00101010200103 ——DD1*19T 20 40 60 80 100 120 140 160 180 200 220 240 260 280 m/z 57.10 93.46%

Abundance #190569: 1-Octadecene (CAS) $$ .alpha.-Octadecene $$ Octad... 57 83

4

5000 111 25.80 26.00 26.20 26.40 m/z 83.10 85.42% 116 । 153168 196 224 252 01 , , , I ! , j J — ...M rn/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #195644:1-Heptadecanol $$ n-Heptadecanol $S Heptadecyl al... 55 83 T T T T 25.80 26.00 26.20 26.40 5000 m/z 69.10 71.82%

JU 111

4 126 a 154 182 210 238 01 TTmPumouana—neeagu miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #226374:5-Eicosene, (E)- 55 T T T 25.80 26.00 26.20 26.40 m/z 97.10 65.73% 83 5000

29 111

m/z—> 0 ' I 4 4 14 —r 126 , 153168 196 224 252 280 । fi 11”]' i ■ i"i । il 11 |'i i > i j 1111111111111111 > 11111 20 40 60 80 100 120 140 160 180 200 220 240 260 280 ' ■ i ■ ■ ■ ■ i • ■ ■ • i ■ • ‘ ■ i ■ • 25.80 26.00 26.20 26.40

7115.D 5080402BBC.M Tue Apr 23 15:52:52 2002 Page 7

NYC-WTC_000049084

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NYC-WTC_000049084Source: NYC Law Department, mirrored locally

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