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GCMS sample AE07110 results, April 25, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis results for sample AE07110 including detection of unknown compounds.

NYC-WTC_000049027–000049062

Folder label: “GCMS X 4/12/02 A 4/23/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohik Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 Nonadecane Concentration Rank 17

R.T. EstConc Area Relative to ISTD R.T.

25.07 2.19 ug/L 283045 Phenanthrene-dl0 22.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Nonadecane 268 C19H40 000629-92-5 90 2 Iron, tricarbonyl[N-(phenyl-2-py... 398 C21H14FeN2O3 074764-11-7 83 3 Octadecane 254 C18H38 000593-45-3 83 4 Hexadecane (CAS) $$ n-Hexadecane... 226 C16H34 000544-76-3 78 Abundance Scan 3743 (25.072 min): 7110.D (-) m/z 57.10 100.00% 57

5000 85 Aww 4'I 24.80 25.00 25.20 25.40 1p0 126141 177 Of T[‘ -HAH4rH*i F> fit । rfi Mi । fi 11'| । ■ 11111।।।. m/z 71.10 55.29% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #211481: Nonadecane 57

AWWV 5000 4I 85 24.80 25.00 25.20 25'40 m/z 43.10 49.50% 1 113 Of fuimp .4.A. 4,, A 141 4 199 . 196211 r, 239, ..268.., 20 40 60 80' ‘lOO 120 140 160 186' 200 220 240 ‘260’ 280 rn/z-> Abundance #331028: Iron, tfcarbonyl[N-(phenyi-2-pyridinylmethytene).,. 57 Www 25.00 26'2636.48% m/z24.8085.10 25.40 5000 85

4

m/z-> 0

Abundance 20 40 24.4444113411160,197.,225.,,253/.282. 60 80 100 120 140 160 180 200 220 240 260 280 #193178: Octadecane AYhush 57 24.80 25.00 25.20 25.40 m/z 55.10 24.37%

5000 41 85 AMWo 28 . i A j. J 1141,169 . 197 225 2?4 0 -mrmmmmpTppt 24.80 25.00 25.20 25.40 m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280

7110.D 5080402BBC.M Tue Apr 23 15:52:14 2002 Page 8

NYC-WTC_000049047

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NYC-WTC_000049047Source: NYC Law Department, mirrored locally

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