GCMS analysis report for sample AE07382, April 2002

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Data File : C:\MSDCHEM\l\DATA\041802\7382.D Vial: 31 Acq On : 19 Apr 2002 10:16 am Operator: Bohlk Sample : SAMPLE 7382 3/28/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 Nonadecane (CAS) $$ n-Nonad... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

23.85 1.07 ug/L 117986 Phenanthrene-dlO 22.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Nonadecane (CAS) $$ n-Nonadecane 268 C19H40 000629-92-5 78 ■ 2 Pentacosane $$ n-Pentacosane 352 C25H52 000629-99-2 78 3 Hexacosane $$ n-Hexacosane 366 C26H54 000630-01-3 78 4 Tricosane (CAS) $$ n-Tricosane 324 C23H48 000638-67-5 72 Aibundance Scan 3535 (23.849 min): 7382.D (-) m/z 57.10 100.00% 57

5000 85

23.60 23.80 24.00 24.20 0 J 188 m/z 71.10 53.70% ■n/z-> 50 100 150 200 250 300 350 Abundance #211483: Nonadecane (CAS) $$ n-Nonadecane 57

5000 85 23.60 23.80 24.00 24.20 m/z 43.10 44.77% ■I J 169.197 225 268 0 . I I \ T . . q ... t I . . . ‘l < 1'1 I I 1 S Tl/Z-> 50 100 150 200 250 300 350 Abundance #300501: Pentacosane $S n-Pentacosane 57

23.60 23.80 24.00 24.20 5000 m/ Z 85.20 35.75% 85

m/z-> 0

Abundance IkUM 50 100 150 200 250 300 #311169: Hexacosane $$ n-Hexacosane 350 I I S7 23.60 23.80 24.00 24.20 m/z 41.20 21.14%

5000 85

■n/z-> 0 50 100 150 200 250 300 350 366 UUiWWU 23.60 23.80 24.00 24.20

7382.D 5080402BBC.M Tue Apr 23 19:05:16 2002 Page 4

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