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Sample AE10187 analysis results, May 2002

Machine-extracted title · confidence 90%

Analytical results for sample AE10187 analyzed on May 6, 2002, listing compounds detected below the method detection limit.

NYC-WTC_000082581–000082617

Folder label: “525 X 4/30/02 A 5/1/02

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Scanned page image, NYC-WTC_000082606
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050202\10187.D Vial: 23 Acq On 2 May 2002 7:46 pm Operator: Bohlk / Inst 213 Sample SAMPLE 10187 4/30/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

QuantiMethod : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 C33 botryococcane (9) Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

23.53 0.10 ug/L 224082 Phenanthrene d-10 21.89

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 C33 botryococcane (9) 465 C33H68 000000-00-0 86 2 Eicosane (CAS) $$ n-Eicosane 282 C20H42 000112-95-8^$8^ 3 Docosane (CAS) $$ n-Docosane $$ ... 310 C22H46 000629-97-0 72 4 Hexacosane $$ n-Hexacosane 366 C26H54 000630-01-3 72 Abundance Scan 1373 (23.529 min): 10187.D (-) m/z 71.10 100.00% Th

5000 gg

127 155 , 203 23.20 23.40 23.60 23.80 353 m/z 85.05 75.26% 0 m/z-> 50 100 15O__J0p__J50___300__J15g^^ (Abundance #359690: C33 botryococcane (9) 85

113 5000 141 23.20 23.40 23.60 23.80 169 224 m/z 57.10 62.09%l 197 294 ... I 323 351 379 4^ 462 oH- m/z-> 50 100 150 200 250 300 350 400 450 Abundance #228990: Eicosane (CAS) $5 n-Eicosane 57

23.20 23.40 23.60 23.80 5000 m/z 99.10 45.20% 85

i rjV?\l69l?7 225 253 ____________ L.__ o Ha m/z-> 50 100 150 200 ' 250 300 ' 350 400 ' 450 <kbundance#261317: Docosane (CAS) $S n-Docosane $$ C22H46 STANDARD $... 517 23.20 23.40 23.60 23.80 m/z 127.20 24.32%

85 5000

113 310 0^ Tl/2-> 50 100 150 200 250 300 350 400 450 23.20 23.40 23.60 23.80

10187.D 050102.M Mon May 06 15:08:12 2002 Page 15

NYC-WTC_000082606

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NYC-WTC_000082606Source: NYC Law Department, mirrored locally

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