Water quality monitoring data sheet, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051302\11311.D Vial: 13 Acq On : 13 May 2002 9:36 pm Operator: Bohlk / Inst 213 Sample : SAMPLE 11311 5/10/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\050802.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L

Peak Number 18 [1,1’-Biphenyl]-4,4'-diamin... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. (. ree 26.65 4.63 ug/L 4016900 p-Terphenyl d-14 27.42

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 [1,1'-Biphenyl]-4,41-diamine, 3,... 212 C14H16N2 000612-82-8 72 2 [2.2](2,6)pyrazinophane 212 C12H12N4 123624-86-2 64 3 Benzenamine, 2-methoxy-N-(3-pyri... 212 C13H12N2O 041855-67-8 59 4 Benzenamine, 2-methoxy-N-(4-pyri... 212 C13H12N2O 041855-68-9 59 Abundance Scan 1717 (26.649 mln): 11311.D (-) m/z 212.20 100.00% 2 2

5000

106 26.40 26.60 26.80 27.00 0- 52 66 78 92 J 124136 156 168 180 194 . m/z 106.10 20.77% I 1" l 1’4’ 1 I ' 1 i"I 1 1’i ' "I 1 * 1 1 1 1 । n/z-> 40 60 80 100 120 140 160 180 200 220 Abundance #133761: [1,1’-Biphenyl]-4,4’-diamine, 3,3’-dimethyl-, dih... 2 12

5000 pmmmm 26.40 26.60 26.80 27.00 m/z 211.20 16.79%

0- • • 42 77 106 i • ■ • < । > • • » । 1 ■■ 1 I «•> * > I > 130141152 168180 196 . m/z-> 40 60 80 100 120 1140 160 180 200 220 Abundance #132924: [2.2](2,6)pyrazinophane 2 2

26.40 26.60 26.80 27.00 5000 m/z 213.20 16.66%

158 185

miz-> Abundance 0- 40 60 80 100 120' 140 144 t .... l[l, , 171

160 180 200 220 #133320: Benzenamine, 2-methoxy-N-(3-pyridinylmethylene)-... I x mmmmmp 212 26.40 26.60 26.80 27.00 m/z 208.20 15.94%

5000 80 105 51 65 93 11 120 134 181 197 168 0 • 1 i ■ ■ 113 —————————— 1 11« । mi 11 ■ 1 FPt m/z—> 40 60 80 100 120 140 160 180 200 220 26.40 26.60 26.80 27.00

L1311.D 050802.M Tue May 14 11:10:50 2002 Page 20

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