Water quality monitoring data sheet, May 2002

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Data File : C:\MSDCHEM\l\DATA\051302\11311.D Vial: 13 Acq On : 13 May 2002 9:36 pm Operator: Bohlk / Inst 213 Sample : SAMPLE 11311 5/10/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\050802.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L

Peak Number 17 3-(4-Hydroxy-3-nitrophenyl)... Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

26.43 0.07 ug/L 60105 p-Terphenyl d-14 27.42

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-(4-Hydroxy-3-nitrophenyl)pyridine 216 C11H8N203 000000-00-0 53 2 1-(6-Methoxymethylnaphthalen-2-y... 216 C14H1602 118513-22-7 53 3 Thianthrene $$ Thianthren $$ Thi... 216 C12H8S2 000092-85-3 53 4 IIH-Benzo[a]fluorene $$ Benzo[a]... 216 C17H12 000238-84-6 53 Abundance Scan 1693 (26.432 min): 11311.D (-) m/z 216.10 100.00% 2 6

5000 108 170 TT-p-T ■ ■ i' 1 ■ ■ i • ■

55 71 85 26.20 26.4026.60 26.80 0- l ' • ' • t ' * ' Il' I 1 'III‘ ' I *I ' • i ' I • a1t.............. .. .... nl j m/z 108.00 27.81% rn/z-> 20 40 60 80 100 120 140 160 180 206’ 220 Abundance #138069:3-(4-Hydroxy-3-nitropheny!)pyridine 2 6

5000 T T T 26.20 26.40 26.60 26.80 170 m/z 170.10 25.15%

miz-> 0-1 20 .. 43,457,471,48203 129.711,158) 180183 "266' 40 60 80 100 120 199 140 160 i ' 1 220 Abundance #138945: 1-(6-Methoxymethylnaphthalen-2-ylethanol 45 ’ I’* 1 ' ' ' 1 ' ’ I’’ 216 26.20 26.40 26.60 26.80 141 m/z 217.20 17.38% 5000 201

171 185

rn/z-> 0, “I ■ 31 20 , .63 77 89 101 115 4 1 155 a 1711′1 “i । |“r i-i"i“ । i”i"i ‘Tt । । >Ti । T — 40 60 80 100 120 140 160 180 200 220 U48

Abundance #138359: Thianthrene $$ Thianthren $$ Thiaanthrene $$ 9,10... 216 26'20 26.40 26'60 26.80 m/z55.10:11.17%

m/z—> 5000

28 45 57 69 82 96 198 127 | 152 0-TTTTT------i 20 40 60 , 80 100 120 140 160 180 139 171 184

203 J 200 220 4 meww WWa 1 ■ i ■ ■ • ■ i • ■ ■ • j < • 26.20 26.40 26.60 26.80

1311.D 050802.M Tue May 14 11:10:49 2002 Page 19

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