GCMS surrogate recovery results, sample AE07110, April 15, 2002

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. Data File : C:\MSDCHEM\l\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohlk Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title Quantitation For Method 508gcscan Library C:\DATABASE\WILEy7N.L

Peale Number 10 Heptacosane Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

27.37 .12.57 ug/L 1508300 Chrysene-dl2 30.14

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Heptacosane 380 C27H56 000593-49-7 91 2 Tricosane (CAS) $$ n-Tricosane 324 C23H48 000638-67-5 91 3 Eicosane 282 C20H42 000112-95-8 91 4 Pentadecane 212 C15H32 _____ 000629-62-9 87 Abundance Scan 4135 (27.375 min): 7110.D (-) m/z 57.10 100.00% 7

5000 85

■n" J 27.00 27.20 27.40 27.60 J i 197 225 253 m/z 71.10 60.13% 0^ 'n/z-> 100 150 200 250 300 350 Abundance #320678: Heptacosane 57

5000 85 27.00 27.20 27.40 27.60 m/z 43.15 44.84%

■n/z-> Oi XUi 50 100 150 •»69J 97 225 253 281 309 337 200 ' 250 300 350 380

Abundance #275685: Tricosane (CAS) $S n-Tricosane 57

"T 27.00 27.20 27.40 27.60 TiTiTil 85 m/z 85.10 42.53%

28 ills > . i J , JJ I 239 267,295 324 0 -n/z-> 50 100 150 200 250 300 350 Abundance #228992: Eicosane 5|7 "n" 27.00 27.20 27.40 27.60 m/z 55.10 20.00%

5000 85 29

0 I jT,141 169 I ' ' ' * i' ■' ' 282 m/z-> 50 100 150 200 250 300 350 27.00 27.20 27.40 27.60

7110.D 5080402BB.M Mon Apr 15 17:09:19 2002 Page 12

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