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GCMS sample AE07115 results, April 25, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis results for sample AE07115 including detection of unknown compounds.

NYC-WTC_000049063–000049101

Folder label: “GCMS X 4/12/02 A 4/23/02

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NYC 9/11 Public Portal Document Library Search Compound Report

. Data File : C:\MSDCHEM\1\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohik Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 7 Cyclohexanone, 4-(1,1-dimet... Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

27.77 16.34 ug/L 2000030 Chrysene-d12 30.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexanone, 4-(1,1-dimethylpr... 168 C11H20O 016587-71-6 25 2 Heptadecane, 4-propyl- $$ 4-n-Pr... 282 C20H42 055044-10-5 22 3 Heptadecane (CAS) $$ n-Heptadeca... 240 C17H36 000629-78-7 20 4 Piperidine, 4-methyl- (CAS) $$ 4... 99 C6H13N 000626-58-4 18 Abundance Scan 4202 (27.769 min): 7115.D (-) m/z 57.10 100.00% 57 43 104 71 5000 85 ' i ■ ■ ■ ■ i ■ ■1 ■ i • • ‘ ‘ i • ■ ■ • i • 239 27.40 27.60 27.80 28.00

m/z—> 0 T40 20 l4.‘21(015416812.,208,225.4.257 60 80 100 120 140 160 180 200 220 240 260 m/z 43.10 77.07%

Abundance #71139: Cyclohexanone, 4-(1,1-dimethylpropyl)- $$ Cyclohex... 71 98

55 5000 27.40 27.60 27.80 28.00 T 4 m/z 55.10 74.42%

n/z—> 0 274444441139553/4. 20 40 60 80 100 120 140 160 180 200 220 240 260 TTTT Abundance #228981: Heptadecane, 4-propyl- $$ 4-n-Propylheptadecane 57 43 27.40 27.60 27.80 28.00 1 5000 m/z 104.10 64.07% 71 29 85 99 239 t .1 113127141155169183197211225 1 253 0111 ‘ 1 ‘ T ’ "T ’ 1 . |T. » । | . it 11 ri > i 1 >‘I I m 1 |11 1114 n | | I I I i'1)'1 1 ' ' I ’’ miz—> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #174553: Heptadecane (CAS) $$ n-Heptadecane $$ Normal-hept... 43 57 ■ i ■ ■1 • i • • • • i ifffer 111 r 27.40 27.60 27.80 28.00 m/z 98.10 59.05% 71 5000 85 29 99

m/z-> 0 20 4 40 ............................. ..... 60 80 100 120 140 160 180 200 220 240 260 PV IT T T T 27.40 27.60 27.80 28.00 TT

7115.D 5080402BBC.M Tue Apr 23 15:52:56 2002 Page 10

NYC-WTC_000049087

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NYC-WTC_000049087Source: NYC Law Department, mirrored locally

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