GCMS surrogate recovery results, sample AE07110, April 15, 2002

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Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohlk Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 Benzene, (1,3,3-trimethylno... Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

22.63 2.60 ug/L 335968 Phenanthrene-dl0 22.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzene, (1,3,3-trimethylnonyl)- 246 C18H30 054986-44-6 72 2 Hexacosane 366 C26H54 000630-01-3 47 3 Octacosane 394 C28H58 000630-02-4 43 4 Eicosane (CAS) $$ n-Eicosane 282 C20H42 000112-95-8 43 Abundance Scan 3328 (22.633 min): 7110.D (-) m/z 105.10 100.00% 105

57 5000

22.40 22.60 22.80 23.00 J. 246 m/z; 57.10 53.25% 0 m/z-> 50 100L.. .150 200 250 300 350 Abundance #182126: Benzene, (1,3,3-trimethyinonyl)- 105

5000 22.40 22.60 22.80 23.00 57 “in/z 71710 37727%

29 127 161 190 246 0 I -n/z-> 50 100 150 200 250 300 350 Abundance #311167: Hexacosane . 57

22.40 22.60 22.80 23.00 5000 m/z 43.10 24.59%

'''W 85

29D .. . 0 ' ' ' I ' ■n/z-> 50 100 150 200 250 300 350 Abundance #329267; Octacosane 57 22.40 22.60 22.80 23.00 m/z 85.10 22.04%

5000 85

29 0 J I 253 281 309 337 365 394 Tl/Z-> 50 100 150 200 250 300 350 22.40 22.60 22.80 23.00

110.D 5080402BB.M Mon Apr 15 17:09:11 2002 Page 5

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