GCMS surrogate recovery results, sample AE07110, April 15, 2002

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Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohlk Sample : S7U4PLE 7110 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title Quantitation For Method 508gcscan Library C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 Heptacosane Concentration Rank 19

R.T. EstConc Area Relative to ISTD R.T.

21.79 1.22 ug/L 156756 Phenanthrene-dl0 22.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptacosane 380 C27H56 000593-49-7 43 2 Eicosane 282 C20H42 000112-95-8 43 3 butyl 2,4-dimethyl-2-nitro-4-pen... 229 C11H19NO4 113747-73-2 38 4 Undecane, 3,5-dimethyl- (CAS)______ 184 C13H28 017312-81-1 38 Abundance Scan 3184 (21.787 min): 7110.D (-) m/z 57.10 100.00%

% M 5(7 91

5000

133 112 0 I o nJ I I I 21.40 21.60 21.80 22.00 22.20 m/z 91.10 93.03% •n/z-> 50 100 150 200 250 300 350 Abundance #320678: Heptacosane 57

SEE 85 21.40 21.60 21.80 22.00 22.20 m/z 71.10 59.28% 29 i I ■I I 1 |113 ,141,169 197 225 253 281 309 337 380 0 m/z-> *50 100 15O____JOO___25O_^^ Abundance #228992: Eicosane 57

21.40 21.60 21.80 22.00 22.20 5000 m/z 43.10 40.00% 85 29

oi 1 PP,141 169 282 m/z-> 50 100 150 200 250 300 350 Abundance #158031: butyl 2,4-dimethyl-2-nitro-4-pentenoate 5f7 21.40 21.60 21.80 22.00 22.20 m/z 85.10 38.50%

m/z-> SEEl

0 “I 50 85

100 113

150 212 200 250 300 350 J 21.40 21.60 21.80 22.00 22.20

7110.D 5080402BB.M Mon Apr 15 17:09:10 2002 Page 4

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