GCMS sample AE07110 results, April 25, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report . Data File : C:\MSDCHEM\l\DATA\041002\7110.D vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohik Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 2 Heptacosane Concentration Rank 19

R.T. EstConc Area Relative to ISTD R.T.

21.79 1.22 ug/L 156756 Phenanthrene-dl0 22.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptacosane 380 C27H56 000593-49-7 43 2 Eicosane 282 C20H42 000112-95-8 43 3 butyl 2,4-dimethyl-2-nitro-4-pen... 229 C11H19NO4 113747-73-2 38 4 Undecane, 3,5-dimethyl- (CAS) 184 C13H28 017312-81-1 38 Abundance Scan 3184 (21.787 min): 7110.D (-) m/z 57.10 100.00%

« M 57 91

5000 W 133 112 21.40 21.60 21.80 22.00 22.20

m/z-> 0- LMILLLL 50 100 150 200 250 300 ' 350' m/z 91.10 93.03%

Abundance #320678: Heptacosane 57

5000 hapha 4 21.40 21.60 21.80 22.00 22.20 85 m/z 71.10 59.28% 29 0- r i 1 1,41134141.169 197 225,253 281 309 337,380 * -n/z-> 50 ' ' '160' ' ' 150 ‘ ' 260' ' ' ‘25o‘ ' ‘ 360' 350 Abundance #228992: Eicosane 57

21.40 21.60 21.80 22.00 22.20 m/z 43.10 40.00%

yAlr 5000 85 29

0- ■ ■ r 1i .113,141 189 .. 1 282 > "r ■ | 1 ■ ■ r | > ' 1 1 | miz-> 50 100 150 200 250 300 350 Abundance #158031: butyl 2,4-<jlmettiyl-2-nitro-4-pentenoate 57 21.40 21.60 21'80 22.00 22.20 m/z 85.10 . 38.50%

5000

85

. 113 212 0 • • । • i • • • । • • ■ ■ i • i ■ 1 1 * • i' ■ • ■ i T T IEt rn/z-> 50 100 150 200 250 300 350 21.40 21.60 21.80 22.00 22.20

7110.D 5080402BBC.M Tue Apr 23 15:52:09 2002 Page 4

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