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GCMS sample AE07110 results, April 25, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis results for sample AE07110 including detection of unknown compounds.

NYC-WTC_000049027–000049062

Folder label: “GCMS X 4/12/02 A 4/23/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohlk Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 18

R.T. EstConc Area Relative to ISTD R.T.

11.93 2.05 ug/L 234655 Naphthalene-d8 12.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 59 3 Pentasiloxane, 1,1,3,3,5,5,7,7,9... 356 C1OH32O4S15 000995-83-5 40 4 1,2-BIS(TRIMETHYLSILYOXY)-4-TRIM... 356 C16H3203Si3 000000-00-0 38 Abundance Scan 1506 (11.928 min): 7110.D (-) m/z 73.10 100.00% 73

5000 267 355 IeunamnemomaDTT 11.60 11.80 12.00 12.20 45 I 162 193 m/z 267.00 31.35% 0- 4 i 100 ■ 11** I • 237 1.ki —4 tn/z-> 50 150 200 250 300 350 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 11.6011.80 12.00 12.20 m/ z 35 5.0 0 17.83% 45 207 323 0- | ii "R ■ i 1 ■ • ■ i ■ • । । । T ' 1** I** m/z-> 50 100 150 200 250 3001 350 Abundance #313065: Cyclopentasiloxane, decamethyl- 73 ‘TT — T T 11.6011.8012.0012.20 m/z74.10 8.14% 5000 267 355 45 .1 i 133 165,1934,223 247.4 293 323 . 4 . 0- *261 ‘ 96 ‘ i • ‘ m/z-> 50 100 150 200 250 300 350 Abundance #302654: Pentasiloxane, 1,1,3,3,5,5,7.7,9,9-decamethyl- 73 267 ‘‘12211119 i • •' ■ i ■ ■ ■ • i 11.6011.8012.00 12.20 m/z59.10 7.81%

133 5000 341 207 45 | 0 — —++ 41771/4,2274,4 103 • 309 i • ■ ’ i ‘ ■ m/z—> 50 100 150 200 250 300 350 11,6011.80 12.00 12.20

7110.D 5080402BBC.M Tue Apr 23 15:52:08 2002 Page 3

NYC-WTC_000049042

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NYC-WTC_000049042Source: NYC Law Department, mirrored locally

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