GCMS analysis results for sample AE06095, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\040402B\6095.D vial: 18 Acq On 5 Apr 2002 9:25 am Operator: Bohlk Sample SAMPLE 6095 3/15/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L .

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.97 0.67 ug/L 363108 Naphthalene-d8 12.94

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Cyclopentasiloxane, decamethyl - 370,ci0H30O5Si5 000541-02-6 59 3 l,3-BIS(TRIMETHyLSILYLOXY)-2-TRI... 573 C24H51NO5Si5 000000-00-0 38 4 Benzeneacetic acid, .alpha.,4-bi... 326 C15H26O4Si2 055334-40-2 37 Abundance Scan 1513 (11.969 min): 6095.D (-) m/z 73.10 100.00% 73 I 5000

267 T 355 IM 193 .^7^ 1 ,, .................. 11.60 11.80 12.00 12.20 0 m/z 267.00 21.56% ■n/2-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 11 60 11.80 12.00 12.20 m/z 355.10 14.60%

[n/z-> Abundance 01 I ! 'I ' 50 100 207 ■ I '■ , ' T 150 200 250 300 350 400 450 323 T' ’ I #313065: Cyclopentasiloxane, decamethyl- 500 550 I 73

. ................... 11.60 11^80 12,00 12.20 5000 m/z 74.10 8.74% 267

355

28! , 1O3133163,1?3223 , 323 0 -rm-r -n/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #379385: 1,3-BIS(TRlMETHYLSILYLOXY)-2-TRIMETHYLSILYLAMiNO- 70 11.60 11.80 12.00 12.20 m/z 356.00 6.57%

5000 355

4^ il03 79 218251, 2^”'325 396 440470 530560 0 ' ' I ' ' ' ' I ' ' ’ ' I ' ‘ ‘ ' I • ' m/z-> 50 100 150 200 250 300 350 400 450 500 550 11.60 11.80 12.00 12.20

5095.D 5080402.M Eri Apr 05 12:52:30 2002 Page 3.

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