GCMS analysis results for sample AE06265, April 2002

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Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\ 04 04 02B\62 65.D Vial: 21 Acq On 5 Apr 2002 11:54 am Operator: Bohlk Sample SAMPLE 6265 3/15/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\59.73N\5080402.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.97 ’0.67 ug/L . 371144 Naphthalene-d8 12.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

T Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 78 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 72 3.1,3-BIS(TRIMETHYLSILYLOXY) -2-TRI... 573 C24H51NO5Si5 000000-00-0 38 4 Benzeneethanamine, N-[(pentafluo... 475 C21H26F5N02Si2 055429-85-1 37 Abundance Scan 1513 (11.969 min); 6265.D (-) m/z 73.05 100.00% 73

5000

267 355 11.60 11.80 12.00 12.20 ,. I f|-. " I —J' ■" I................ oU>J m/z 267.00 24.39% ■n/z~> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313068; Cyclopentasiloxane, decamethyl- 73

355 267 11.60 11.80 12.00 12.20 m/z 355.10 13.50%

207 3^3^ 0 ' \ • •' ’ \ ’ t \ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313065; Cyclopentasiloxane, decamethyl-

11.60 11.80 12.00 12.20 liWil m/z 74.10 8.48% 267 355

103133163,''?^223 323 0 T-p-T-i-Tj4-r+-rp-i--ri TT-r+r ■n/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #379385; 1,3-BIS(TRIMETHYLSILYLOXY)-2-TRIMETHYLSILYLAMINO- 73 11.60 11.80 12.00 12.20 m/z 59.05 5.65%

5000 355

1d7 ji03 I 218251, 396 440470 530560 I 0 I' ''' I ' ’'' I'' '' I' '' ' I '' ' ' I'' .... ■n/z-> 50 100 150 200 250 300 350 400 450 500 550 11.60 11.80 12.00 12.20

5265.D 5080402.M Fri Apr 05 17:24:42 2002 Page 3

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