GCMS analysis results for sample AE06094, April 2002

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Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\040402B\6094.D Vial: 17 Acq On 5 Apr 2002 8:35 am Operator: Bohlk Sample SAMPLE 6094 3/15/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peale Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.97 0.65 ug/L 335187 Naphthalene-d8 12.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 74 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 3 Benzeneethanamine, N-[(pentafluo... 475 C21H26F5NO2Si2 055429-85-1 37 4 Pentasiloxane, 1,1,3,3,5,5,7,7,9... 356 C10H32O4Si5 000995-83-5 33 Abundance Scan 1514 (11.975 min): 6094.D (-) m/z 73.10 100.00% 73

5000

267 355

Ti/z-> Abundance 0 45 50 104 100 154 150 193 223 t-V-Aj-r-T—r 200 250 #313068; Cyclopentasiloxane, decamethyl- 300 X 350 11.60 11.80 12.00 12.20 m/z 267.00 23.37%

7t3

355 267 5000 .......... 11.60 11.80 12.00 12.20 m/z 355.00 19.27% 45 207 323 0 -I—Ar-V-q- ■n/2-> 50 100 150 200 250 300 350 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

I \............ 11.60 11.8012.00 12.20 5000 m/z 268.00 8.34% 267 355 45 0 26 ,.l 96 133 165 293 323 m/z-> 50 100 150 200 250 300 350 . Abundance #362614: Benzeneethanamine, N-[(pentafluorophenyl)methylen... 7|3 11.60 11.80 12.00 12.20 m/z 74.10 8.10%

5000 267 44 104 131151 179 209 237 0 •^'■1 ■ rn/z-> 50 100 150 200 250 300 350 11.60 11.80 12.00 12.20

5094.D 5080402.M . Eri Apr 05 09:27:02 2002 Page 3

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