GCMS analysis results for sample AE06959, April 23, 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041702\6959.D Vial: 13 Acq On : 17 Apr 2002 6:36 pm Operator: Bohlk Sample : SAMPLE 6959 3/25/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.93 1.53 ug/L 178789 Naphthalene-d8 12.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 90 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 72 3 Pentasiloxane, 1,1,3,3,5,5,7,7,9... 356 C10H32O4Si5 000995-83-5 40 4 Benzeneethanamine, N-[(pentafluo... 475 C21H26F5NO2Si2 055429-85-1 33 Abundance Scan 1506 (11.928 min): 6959.D (-) m/z73.10 100.00% vh

5000

154 193 237 267

323 355 [ J 11.60 11.80 12.00 12.20 0^ ' I ‘I '■ ' m/z 267.00 26.61% fn/z-> 50 100 150 200 250 300 350 Abundance #313068: Cyclopentasiloxane, decamethyl- 7P

355 267 Wilil •^7 11.60 11.80 12.00 12.20 m/z 355.10 15.33%

45 207 323 L I 0 'n/z-> 50 100 150 200 250 300 350 Abundance . #313065: Cyclopentasiloxane, decamethyl- 7|3

11.60 11.80 12.00 12.20 5000 m/z74710 8.67% 267 355 45 26 ,1 I 96 133 165 , 223 247 293 323 I 0 •-r’ ■n/z-> 50 100 150200 250 300 350 Abundance #302654: Pentasiloxane, 1.1,3,3,5,5,7,7,9,9-decamethyl- 73 21 7 11.60 11.80 12.00 12.20 m/z 59.10 6.67%

133 5000 341 207 103 309 { II 0 n/z-> 50 100 150 200 250 300 350 11.60 11.80 12.00 12.20

6959.D 5080402BBC.M Mon Apr 22 11:46:27 2002 Page 3

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