GCMS surrogate recovery results, sample AE07110, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohlk Sample : STkMPLE 7110 3/27/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 18

R.T. EstConc Area Relative to ISTD R.T.

11.93 2.05 ug/L 234655 Naphthalene-d8 12.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 59 3 Pentasiloxane, 1,1,3,3,5,5,7,7,9... 356 C10H32O4Si5 000995-83-5 40 4 1,2-BIS(TRIMETHYLSILYOXY) -4-TRIM... 356 C16H32O3Si3 000000-00-0 38 Abundance Scan 1506 (11.928 min): 7110.D (-) m/z 73.10 100.00% 73

5000 267 355 "T 11.60 11.80 12.00 12.20 162 193 m/z 267.00 31735% 0 m/z-> 50 100 150 200 250 300 350 /Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 .................. .......................... 11.60 11.80 12.00 12.20 m/z 355.00 17.83% 45 207 323 .^1 0 —At—T—[-A ■n/z-> 50 100 150 200 250 300 350 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

11.60 11.80 12.00 12.20 tiliia m/z 74.10 8.14% 267

355 45 26 1 I 96 133 165 /^3 223 247 293 323 0 T—t—1—y—r ' i'' ■' ' I' ■*’ r' ■n/z-> 50 100 150 200 250 300 350 Abundance #302654: Pentasiloxane. 1,1,3,3,5,5,7,7,9,9-decamethyl- 73 267 11.60 11.80 12.00 12.20 m/z 59.10 7.81%

133 5000 341 207

0 ?l 103 54 177 a [ 237 I# 309 •n/z-> 50 100 150 200 250 300 350 11.60 11.80 12.00 12.20

7110.D 5080402BB.M Mon Apr 15 17:09:09 2002 Page 3

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