GCMS surrogate recovery results, sample AE07111, April 16, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\7111.D Vial: 18 Acq On : 11 Apr 2002 4:01 am Operator: Bohlk Sample : SAMPLE 7111 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\MSDCHEM\l\5973N\5080402BB,M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Pealt Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.92 1.96 ug/L 254584 Naphthalene-d8 12.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 91 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 3 Benzoic acid, 2-[(trimethylsilyl... 282 C13H22O3Si2 003789-85-3 50 4 Benzeneethanamine, N-[(pentafluo... 475 C21H26F5NO2Si2 055429-85-1 50 Abundance Scan 1505 (11.922 min): 7111 .D (-) m/z 73.10100.00% 73

5000

267 355 11.60 11.80 12.00 12.20 0 I 117^ 1^ 193 223 , I , 323 t m/z 267.00 26.86% fn/z-> 50 100____ 150____ 200____ 250_____ 300 350 Abundance #313068: Cyciopentasiioxane, decamethyl- 73

355 267 \ 5000 11.60 11.80 12.00 12.20 m/z 355.00 13.91% 45 207 0 A-v ' I ' .L ''''11' Ti/z-> 50 100 150 200 250.300 350 Abundance #313065: Cyclopentasiloxane, decamethyl- 70 __ 11.60 11.80 12.06 iz20 m/z74.10 S.SO? 5000 267

355 45 96 133 165/*^^ 223 247 293 323 0 m/z-> 50 100 150 200 250 300 350 Abundance #227685: Benzoic acid, 2-[(trimethylsilyl)oxy]-, trimethyl... 7|3 11.60 11.80 12.00 12.20 m/z 268.00 6.56%

5000 267 45

■n/z-> 0 Jk 50 100 135

150 200 233 250 300 350 11.60 11.80 12.00 12.20

7111.D 5080402BB.M Mon Apr 15 17:47:58 2002 Page 3

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