GCMS analysis results for sample AE06963, April 23, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041702\6963.D Vial: 17 Acq On : 17 Apr 2002 9:55 pm Operator: Bohlk Sample : SAMPLE 6963 3/25/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5O8O4O2BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peale Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.93 2.07 ug/L 241896 Naphthalene-d8 12.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 80 2 Benzeneacetic acid, .alpha.,4-bi... 384 C17H32O4Si3 037148-64-4 38 3 Pentasiloxane, 1,1,3,3,5,5,7,7,9... 356 C10H32O4Si5 000995-83-5 33 4 1,2-BIS(TRIMETHYLSILYOXY)-4-TRIM. .. 356 C16H32O3Si3 000000-00-0 32 Abundance Scan 1506 (11.928 min): 6963.D (-) m/z 73.10 100.00% 73

5000 267 355 l""i 11.60 11.80 12.00 12.20 45 , 125 162 193 323 m/z 267.00 30.72% 0 I I ■' I 'I ' ' ' ' I ' m/z-> 50 100 150 200 250 300 350 400 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

5000 267 11.6011.80 12.00 12.20 355 m/z 355.00 17.85% 45 133,165 ''^^ 223244 0^ Jl 96 293 323 I ■n/z-> 50 100 150 200 250 300 350 400 Abundance #322334: Benzeneacelic acid,.alpha.,4-bis[(tnmethylsilyt... 73 267

11.60 11.80 12.00 12.20 tililil m/z 268.00 8.59%

45 147 105126 L 168/^^214237, 341 296317 t ^^^390 0 ' I ' ' ' ' I '■ ' ' ' I I r I 'I r ■n/z-> 50 100 150 200 250 300 350 400 Abundance #302654: Pentasiloxane, 1,1,3,3,5,5,7,7,9,9-decamethyl- 73 267 11.60 11.80 12.00 12.20 m/z 74.10 8.34%

133 5000 341 207 45 . 154,237^1 103 0 I 309 ■*T ■n/z-> 50 100 150 200 250 300 350 400 11.60 11.80 12.00 12.20

6963.D 5080402BBC.M Mon Apr 22 12:29:33 2002 Page 3

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