GCMS analysis results for sample AE06093, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\040402B\6093.D Vial: 16 Acq On 5 Apr 2002 7:46 am Operator: Bohllc Sample SAMPLE 6093 3/15/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\MSDCHEM\l\5973N\5080402.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N;L ********************************************************************* Peale Number 2 Cyclopentasiloxane, decamet... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.97 0.75 ug/L 395794 Naphthalene-d8 12.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 59 2 3,4-Dihydroxybenzyl alcohol,tris... 356 C16H32O3Si3 068595-79-9 47 3 Benzeneacetic acid, .alpha.,4-bi... 384 C17H32O4Si3 037148-64-4 47 4 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 40 ZKbundance Scan 1513 (11.969 min): 6093.D (-) 73.10 100.00% 73

5000

267 355 11.60 11.80 12.00 12.20 323 [ m/z 267.00 23.87% oi ' ' ' I ' ' ' ' I ' 'n/z-> 50 100 150 200 250 300 350 400 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

5000 267 11.60 11.80 12.00 12.20 355 m/z 355.00 13.94%

•n/z-> Abundance 0 -4 100 96 133 165 1^ 223

150 200 250 ।

300 293 323 ' ' I ' r ' ’ I . ' ' ' I ' 350 #302823: 3,4-Dihydroxybenzyl alcohol,tris(lrimethylsilyl)- 73 400

......................... / ,1,,,, I,

11.60 11.80 12.00 12.20 267 m/z74710 8.64% 5000 179 356 45 147 15 103 I 209 237 312 , 0 * r' ■n/z-> 50 100 150 200 250 300 350 400 Abundance #322334: Benzeneacetic acid, .aipha.,4-bis((trimethylsilyl... 7(3 267 ' I ' ' ..... I.............. 11.60 11.80 12.00 12.20 m/z 356.00 6.12%

5000

45 147 105 , [ 169^^215237 341 0 296318 L 369392 ■n/z-> 50 100 150 200 250 300 350 400 11.60 11.80 12.00 12.20

6093.D 5080402.M Fri Apr 05 09:14:41 2002 Page 4

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