GCMS analysis results for sample AE06266, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\040402B\6266.D ■ Vial: 22 Acq On 5 Apr 2002 12:43 pm Operator: Bohlk Sample SAMPLE 6266 3/15/02 Inst : Instruraen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\i\5973N\5080402.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.97 0.48 ug/L 255984 Naphthalene-d8 12.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 3 3,4-Dihydroxybenzyl alcohol,tris... 356 C16H32O3Si3 068595-79-9 43 4 Heptasiloxane, 1,1,3,3,5,5,7,7,9... 504 C14H44O6Si7 019095-23-9 36 Abundance Scan 1514 (11.975 min): 6266.D (-) m/z 73.10 100.00%! 7P

5000

267 355 1111111111111 > 1111111 V 45 11.60 11.80 12.00 12.20 01 133 1^ 193 ^ , , , , A 323 I m/z 267.00 24798% mZz-> 50 100 150 200 250 300 350 (Kbundance #313068: Cyclopentasiloxane, decamethyl- Tb

355 267 5000 'I ri I I I I I I I I I I I I I I I I I 11.60 11.80 12.00 12.20 m/z 355.00 15.25%!

45 207 01 n • ' r’ I I 50 100 150 200 250 300 350 (\bundance #313065: Cyclopentasiloxane, decamethyl- 73

11.60 11.80 12.00 12.20 5000 m/z 356.00 8.0^ 267 355 45 96 133 165 J 223 2^ t, ,293 323 | oi •n/z-> . 50 100 150 200. 250 300 350 Abundance #302823: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 1 p I I'l I I I I I I I I I I I I I I 7|3 11.60 11,80 12.00 12.20 m/z74710 7.44%i

5000 179 267

356 I 45 147 I'- \ r 0 i 103 , 209 237 , I '^1 f*' I n ■n/z-> 50 100 150 200 250 300 350 11.60 11.80 12.00 12.20

266.D 5080402.M Fri Apr 05 17:29:19 2002 Page 3

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