GCMS analysis results, sample AE06857, April 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041702\6857.D Vial: 6 Acq On : 17 Apr 2002 12:43 pm Operator: Bohlk Sample : SAMPLE 6857, FB 3/25/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number T Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.93 1.27 ug/L 197569 Naphthalene-d8 12.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 2 Cyclopentasiloxane,, decamethyl- 370 C10H3005Si5 000541-02-6 64 3 3,4-Dihydroxybenzyl alcohol,tris... 356 C16H32O3Si3 068595-79-9 47 4 M-HYDROXYPHENETHANOL 2TMS 282 C14H26O2Si2 000000-00-0 28 Abundance Scan 1506 (11.928 min): 6857.D (-) m/ z 73.10 100.00% 7)3

TiWil

267

X 355' 11.60 11.80 12.00 12.20 45 IM 193,223 ,,, m/z 267.00 25,61% m/z-> 0l -M- 50 100 i'' ' ' 150 200 I ■’ I 250 300 350 Abundance #313068: Cyclopentasiloxane, decamethyl- 7j3

355 267 TiTiTil I Y 11.60 11.80 12.00 12.20 m/z 355.10 16.68% 45 323 oi I I—I—rS-V—|-A "0“ in/z-> 50 100 150 200 300 350 Abundance #313065; Cyclopentasiloxane, decamethyl- 73 ............ ,,,,,'............... 11.60 11.80 12.00 12.20 Wilili m/z74710 8.21% 267 355 45 ■I I I J 96 133 165, 223 247 293 323 0 ■n/z-> 50 100 150 200 300 250 350 Abundance #302823: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 70 11.60 11.80 12.00 12.20 m/z 356.00 7.20%

267 5000 179 356 45

m/z-> 0 15 50 103 t-V-yH- 100 X 150 , 209 237 , ' I 200 / , *1 250 312 300 ' I ' 350 11.60 11.80 12.00 12.20

6857.D 5080402BBC.M Mon Apr 22 11:13:44 2002 Page 3

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