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GCMS analysis results for sample AE06091, April 2002

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Laboratory report documenting GCMS analysis of environmental sample AE06091 conducted on April 18, 2002.

NYC-WTC_000060007–000060015

Folder label: “GCMS X 3/15/02 A 4/5/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\040402B\6091.D Vial: 14 Acq On 5 Apr 2002 6:07 am Operator: Bohlk Sample SAMPLE 6091 3/15/02 Inst : Instrunien Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402.M (RTE .Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.97 0.92 ug/L 495158 Naphthalene-de 12.94 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 74 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 50 3 3,4-Dihydroxybenzyl alcohol,tris... 356 C16H32O3Si3 068595-79-9 47 4 1,3-BIS(TRIMETHYLSILYLOXY)-2-TRI... 573 C24H51NO5Si5 OOOOOO-OO'-O 43 /Abundance Scan 1513 (11.969 min): 6091 .D (-) m/z 73.10 100.00% 7)3

5000

267 "T 355 11.60 11.80 12.00 12.20 45 109 133 162 193 223 324 [ m/z 267.00 22.06% Ol-r- -n/z-> 50 100 150 200 250 300 350 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

5000 267 11.60 11.80 12.00 12.20 355 m/z 355.00 16.00% 45 j 133 165 J , 223 247 293 323 0 'I 'n/2-> 50 100 150 200 250 300 350 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 11.60 11.80 12.00 12.20 267 m/z 74.10 6.46% 5000

4.5 323 0 ' I ' I ' •n/z-> 50 100 150 200 250 300 350 Abundance #302823: 3,4-Dihydroxybenzyl alcohol.tris(trimethylsilyl)- 7)3 . ............. 11.60 11.80 12.00 12.20 m/z 75.10 6.11%

TiBIil 267 179 356 45 103 , 209 237 312 0 ’ * i'"' I ‘ m/z~> 50 100 150 200 250 300 350 11.60 11.80 12.00 12.20

5091.D 5080402.M Fri Apr 05 06:57:02 2002 Page 3

NYC-WTC_000060014

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NYC-WTC_000060014Source: NYC Law Department, mirrored locally

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