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GCMS analysis results for sample AE06093, April 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of environmental sample AE06093 conducted on April 18, 2002.

NYC-WTC_000060024–000060033

Folder label: “GCMS X 3/15/02 A 4/5/02

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Scanned page image, NYC-WTC_000060031
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\040402B\6093.D Vial: 16 Acq On .5 Apr 2002 7:46 am Operator: Bohlk Sample SAMPLE 6093 3/15/02 Inst : Instrumen. Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L *★*****★**★******★★*★**★★★★★**★★★*★★*★★★**★***★*★*★*★**★*★★★***★***★* Peak Number 1 2-Pentanone, 4-hydroxy-4-me... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.56 1.28 ug/L 472813 1,4-Dichlorobenzene-d4 9.46

Hit# of 5 Tentative ID MW MolForm CAS# Qual .

1 2-Pentanone, 4-hydroxy-4-methyl-... 116 C6H12O2 000123-42-2 64 2 2-Pentanone, 4-hydroxy-4-methyl-... 116 C6H12O2 000123-42-2 64 3 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 53 4 2-Pentanone, 4-hydroxy-4-methyl-... 116 C6H12O2 000123-42-2 53 Abundance Scan 422 (5.559 min): 6093.D (-) m/z 43.10 100.00% 40

-n/z-> 5000

07 0 50 100 150 101

200 152 250 300 350 400 434 5.20 5.40 5.60 5.80 m/z 59710 I 86.21%

Abundance #16593: 2-Pentanone, 4-hydroxy-4-methyl- (CAS) $S Diaceton... 43

5000 ' ' I ' ' ' ' I ' 5.20 5.40 5.60 5.80 m/z 58.10 40.18% 101

-n/z-> oU4 0 50 100 150 200 250 300 350 Sundance #16599: 2-Pentanone. 4-hydroxy-4-methyl- (CAS) $S Diaceton... 43

5.20 5.40 5.60 5.80 5000 m/z 101.10 24.08%

101 1 ,70,J . ................................... ; ..................... ■n/z-> 0 50 100 150 200 250 300 350 400 Abundance #16600; 2-Pentanone, 4-hydroxy-4-methyl- .................. I Ito 40 ■ I ' ' ' • I ' ' ' ' I ' ' ' ' I ” rr ."p 5.20 5.40 5.60 5.80 m/z41.20 9.44%

5000

15 101 0- m/z-> 0 50 100 150 200 250 300 350 400 5.20 5.40 5.60 5.80

5093.D 5080402.M Fri Apr 05 09:14:40 2002 Page 3

NYC-WTC_000060031

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NYC-WTC_000060031Source: NYC Law Department, mirrored locally

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