GCMS analysis results, sample AE07174, April 25, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\041802\7174B.D vial: 11 Acq On 18 Apr 2002 4:56 pm Operator: Bohlk Sample SAMPLE 7174 3/27/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-me... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.57 260.28 ug/L 24784000 1,4-Dichlorobenzene-d4 9.41

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl-... 116 C6H12O2 000123-42-2 83 2 2-Pentanone, 4-hydroxy-4-methyl-... 116 C6H12O2 000123-42-2 78 3 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 78 4 2-Pentanone, 4-hydroxy-4-methyl-... 116 C6H12O2 _____ 000123-42-2 74 Abundance Scan 424 (5.570 min): 7174B.D (-) m/z 43.10 100.00% 59

9101

101 5.20 5.40 5.60 5.80 6.00 ,3,6,l.l|l,. , , 69 83 m/z 59.10 82.23% Oi .......... ' 1 ' ' ' ' I ' ' ' ‘ I'' 'T' ' " I • ' ' ' I • i " I « ••• 116 •n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #16606: 2-Pentanone, 4-hydroxy-4-methyl- (CAS) $S Diaceton... 413

BlilB 59 5.20 5.40 5.60 5.80 6.00 m/z 58.10 31.97% 101 0^ 36,.I, 66 83 133 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #16613: 2-Pentanone, 4-hydroxy-4-methyl- (CAS) SS Diacelon... 43

"T 59 5.20 5.40 5.60 5.80 6.00 5000 m/z 101.10 21.65% 101

69 .83 II 0 ' i'' ' ' ' I ' •n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #16609: 2-Pentanone, 4-hydroxy-4-methyl- 413 5.20 5.40 5.60 5.80 6.00 m/z 41.10 6.75%

5000 59

31 oo 101 0 .........93 j............................. m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 5.20 5.40 5.60 5.80 6.00

7174B.D 5080402BBC.M Mon Apr 22 18:47:28 2002 Page 3

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